CYCLOLEUCINOL(10316-79-7) ¹³C NMR

Product NameCYCLOLEUCINOL

CAS 10316-79-7

Molecular FormulaC6H13NO

Molecular Weight115.17

InChIInChI=1S/C6H13NO/c7-6(5-8)3-1-2-4-6/h8H,1-5,7H2

InChIKey PDNZJLMPXLQDPL-UHFFFAOYSA-N

SmilesC1(N)(CO)CCCC1

Request For Quotation

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-5770          
1-amino-1-cyclopentanemethanol
C6H13NO             (Mass of molecular ion:    115)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.1
      17.0       1.9
      18.0       9.2
      27.0       4.4
      28.0       7.3
      29.0       2.8
      30.0      12.0
      31.0       3.1
      39.0       5.5
      40.0       1.0
      41.0      15.1
      42.0      11.2
      43.0       3.1
      44.0       3.0
      45.0       2.2
      53.0       1.5
      54.0       5.7
      55.0       3.3
      56.0       9.6
      57.0       2.9
      65.0       1.3
      67.0      17.0
      68.0       5.9
      69.0       3.8
      70.0       1.7
      72.0       3.7
      73.0      12.1
      79.0       1.0
      80.0       1.0
      81.0       1.2
      82.0       3.0
      83.0       1.0
      84.0     100.0
      85.0       6.4
      86.0      13.6
      87.0       3.7
      96.0       1.7
      97.0       1.0
      98.0       7.9

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₁₃ N O	0.044 g : 0.5 ml CDCl₃
1-amino-1-cyclopentanemethanol

    Assign.     Shift(ppm)

      A             3.385
      B             3.30
      C             1.75
      D             1.61
      E             1.42
     
     90MHZ : HSP-02-633

     Hz     ppm     Int.

   1365.84   3.418     34
   1364.26   3.414     40
   1353.03   3.386   1000
   1319.70   3.303    105
    709.35   1.775     51
    707.52   1.771     62
    703.00   1.760    128
    701.66   1.756    137
    698.61   1.749    135
    696.29   1.743    101
    692.99   1.734     90
    689.45   1.726     72
    687.13   1.720     62
    686.40   1.718     63
    682.25   1.708     40
    677.73   1.696     30
    673.58   1.686     30
    670.29   1.678     33
    669.92   1.677     33
    667.60   1.671     35
    666.63   1.669     35
    665.53   1.666     33
    660.89   1.654     78
    659.42   1.650     86
    652.95   1.634    144
    652.10   1.632    144
    647.34   1.620    176
    643.55   1.611    237
    641.36   1.605    315
    639.28   1.600    288
    633.79   1.586     97
    631.35   1.580     75
    628.30   1.573     49
    627.93   1.572     49
    625.61   1.566     36
    624.88   1.564     35
    623.29   1.560     32
    578.74   1.449    110
    576.78   1.444     92
    575.07   1.439    104
    573.24   1.435     74
    569.34   1.425     80
    567.38   1.420    136
    566.77   1.419    137
    564.94   1.414    100
    563.35   1.410     93
    562.01   1.407     93
    560.91   1.404     80
    559.08   1.399     62
    555.66   1.391     31

¹H NMR	89.56 MHz
C₆ H₁₃ N O	0.046 g : 0.5 ml CDCl₃
1-amino-1-cyclopentanemethanol

    Assign.     Shift(ppm)

      A             3.394
      B             2.70
      C          1.73 to 1.34

     Hz     ppm     Int.

    304.00   3.395   1000
    241.94   2.702    877
    160.19   1.789     42
    158.69   1.772     47
    154.63   1.727    108
    153.06   1.710    166
    149.81   1.673    206
    148.75   1.661    231
    146.63   1.638    164
    145.38   1.624    117
    144.38   1.613    137
    141.75   1.583    228
    140.13   1.565    188
    138.44   1.546    138
    136.81   1.528    119
    135.19   1.510     90
    134.00   1.497     88
    133.44   1.490     86
    131.63   1.470     71
    127.94   1.429     31
    125.44   1.401     48
    124.50   1.391     60
    122.81   1.372     37
    121.56   1.358     40

in CDCl3