3-METHYL-1-HEPTANOL(1070-32-2) ¹³C NMR

Mass

MS-IW-3820          
3-methyl-1-heptanol
C8H18O              (Mass of molecular ion:    130)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.5
      27.0      15.2
      28.0       3.8
      29.0      19.8
      31.0      16.3
      39.0      14.3
      40.0       2.6
      41.0      56.6
      42.0      26.1
      43.0      87.1
      44.0       4.7
      45.0       5.4
      46.0       2.0
      51.0       1.3
      53.0       4.9
      54.0       3.6
      55.0      98.5
      56.0      71.7
      57.0      42.9
      58.0       2.0
      59.0       1.2
      67.0       3.5
      68.0       3.5
      69.0      47.9
      70.0     100.0
      71.0      12.9
      72.0       1.3
      73.0       2.2
      81.0       1.2
      82.0       5.4
      83.0      42.2
      84.0      92.0
      85.0      16.7
      97.0       5.8
     112.0       5.5
     162.0       1.9

Assign. Shift(ppm) A *1 3.65 B *1 3.62 C 2.89 D *2 1.59 E 1.53 F *2 1.37 G 1.33 to 1.24 J *3 1.24 K *3 1.14 L 0.89 M 0.885

     Hz     ppm     Int.

   1469.85   3.678     37
   1468.14   3.674     34
   1465.33   3.667     83
   1461.91   3.658     56
   1457.89   3.648    160
   1451.42   3.632    185
   1447.88   3.623     54
   1443.85   3.613     90
   1440.55   3.605     51
   1153.20   2.886    122
    654.54   1.638     37
    649.17   1.625     52
    647.71   1.621     49
    646.73   1.619     44
    641.48   1.606     93
    639.89   1.602     46
    636.23   1.592     75
    634.52   1.588     91
    629.39   1.575    100
    621.83   1.556     83
    617.55   1.546     53
    615.72   1.541     56
    614.99   1.539     55
    610.96   1.529     56
    608.40   1.523     46
    605.59   1.516     41
    604.61   1.513     40
    561.52   1.406     60
    555.42   1.390     55
    553.71   1.386    106
    547.85   1.371    101
    546.26   1.367     79
    542.60   1.358     68
    540.77   1.354    128
    537.84   1.346     77
    535.03   1.339    106
    533.45   1.335     75
    530.27   1.327     74
    526.61   1.318    144
    524.29   1.312    169
    522.71   1.308    163
    521.85   1.306    158
    519.29   1.300    261
    515.63   1.291    250
    513.92   1.286    310
    509.40   1.275    209
    503.78   1.261    146
    499.76   1.251     79
    498.41   1.248     83
    495.36   1.240     53
    493.04   1.234     81
    490.11   1.227     46
    488.40   1.223     31
    485.11   1.214     48
    463.01   1.159     50
    460.69   1.153     35
    457.76   1.146     62
    455.69   1.141     51
    453.98   1.136     51
    450.93   1.129     62
    448.49   1.123     55
    440.92   1.104     34
    362.67   0.908    262
    356.93   0.894   1000
    350.22   0.877    887
    339.48   0.850     34