Borane-methyl sulfide complex(13292-87-0) ¹H NMR

Product NameBorane-methyl sulfide complex

CAS 13292-87-0

Molecular FormulaC2H10BS

Molecular Weight76.97

InChIInChI=1S/C2H10BS/c1-4(2)3/h4H,1-3H3

InChIKey RZQLBDKUAPCFPY-UHFFFAOYSA-N

Smiles[B+3]([H-])([H-])([H-])S(C)C

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¹HNMR

¹³CNMR

IR1

Mass

MS-IW-3829          
borane-dimethyl sulfide complex
C2H6S H3B           (Mass of molecular ion:     76)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.4
      24.0       1.4
      26.0       2.0
      27.0       8.2
      35.0      18.1
      44.0       4.0
      45.0      35.9
      46.0      30.3
      47.0      79.8
      48.0       3.1
      49.0       3.8
      57.0       2.7
      58.0       3.4
      59.0       3.5
      61.0      38.0
      62.0     100.0
      63.0       5.0
      64.0       4.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂ H₆ S	0.05 ml : 0.5 ml CDCl₃
borane-dimethyl sulfide complex

    Assign.     Shift(ppm)

      A             2.264
      B             1.50
     
     J(B-11,B)=104HZ

     Hz     ppm     Int.

    905.03   2.265   1000
    754.76   1.889     21
    754.39   1.888     21
    650.76   1.629     24
    650.27   1.628     24
    545.65   1.366     24
    545.29   1.365     24
    544.80   1.364     24
    544.43   1.363     24
    441.28   1.105     21
    440.67   1.103     21

in CDCl3