p-menth-1-ene-9-ol (13835-75-1) 1H NMR
Product Namep-menth-1-ene-9-ol
CAS13835-75-1
Molecular FormulaC10H18O
Molecular Weight154.24932
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MassMS-NW-7326 (R,R)-(+)-p-menth-1-en-9-ol C10H18O (Mass of molecular ion: 154)
Source Temperature: 220 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 12.3 28.0 2.2 29.0 14.3 31.0 13.0 38.0 1.0 39.0 20.5 40.0 6.5 41.0 36.8 42.0 5.2 43.0 12.4 44.0 1.0 45.0 1.5 50.0 1.6 51.0 5.7 52.0 3.3 53.0 24.2 54.0 4.2 55.0 44.8 56.0 6.3 57.0 4.6 58.0 5.6 59.0 2.3 63.0 1.8 65.0 8.1 66.0 4.0 67.0 62.8 68.0 71.4 69.0 16.8 70.0 3.4 71.0 4.1 77.0 20.5 78.0 4.8 79.0 61.6 80.0 13.8 81.0 46.5 82.0 5.5 83.0 2.7 84.0 3.0 85.0 1.8 91.0 21.0 92.0 12.8 93.0 87.6 94.0 100.0 95.0 69.3 96.0 7.5 97.0 5.4 103.0 1.1 105.0 6.0 106.0 1.9 107.0 53.5 108.0 13.6 109.0 2.4 111.0 1.2 119.0 1.3 121.0 59.5 122.0 7.2 123.0 28.7 124.0 3.3 135.0 1.0 136.0 28.1 137.0 3.7 154.0 25.4 155.0 3.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H18 O 0.05 ml : 0.5 ml CDCl3 (R,R)-(+)-p-menth-1-en-9-ol 
Assign. Shift(ppm)
A 5.362 B *1 3.61 C *1 3.45 D 2.44 G 1.631 M 0.920 M 0.893 includes isomers. partially assigned.
Hz ppm Int.2146.97 5.373 152 2145.63 5.369 166 2144.41 5.366 166 2143.19 5.363 173 2141.85 5.360 170 2140.75 5.357 145 1450.07 3.629 120 1448.36 3.625 90 1444.82 3.616 125 1442.75 3.611 96 1439.58 3.603 167 1437.74 3.598 114 1434.20 3.589 155 1386.96 3.471 82 1384.89 3.466 149 1380.49 3.455 100 1378.30 3.449 154 1376.71 3.445 95 1374.39 3.439 128 1367.68 3.423 112 974.73 2.439 184 776.98 1.945 179 687.01 1.720 134 652.10 1.632 873 631.96 1.582 130 630.74 1.579 154 625.24 1.565 146 624.27 1.563 148 619.38 1.550 137 616.94 1.544 130 536.87 1.344 85 536.01 1.342 74 531.37 1.330 90 530.40 1.328 74 524.41 1.313 80 518.92 1.299 79 370.97 0.929 488 364.38 0.912 499 360.35 0.902 1000 353.76 0.886 998
in CDCl3
liquid film
