4-(Diethylamino)salicylaldehyde(17754-90-4) ¹³C NMR

Product Name4-(Diethylamino)salicylaldehyde

CAS 17754-90-4

Molecular FormulaC11H15NO2

Molecular Weight193.24

InChIInChI=1S/C11H15NO2/c1-3-12(4-2)10-6-5-9(8-13)11(14)7-10/h5-8,14H,3-4H2,1-2H3

InChIKey XFVZSRRZZNLWBW-UHFFFAOYSA-N

SmilesC(=O)C1=CC=C(N(CC)CC)C=C1O

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Mass

MS-NW-7273          
4-diethylamino-2-hydroxybenzaldehyde
C11H15NO2           (Mass of molecular ion:    193)

   Source Temperature: 140 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      27.0       1.9
      28.0       1.1
      29.0       3.3
      39.0       3.9
      42.0       1.1
      51.0       1.3
      52.0       1.0
      53.0       1.7
      63.0       1.7
      64.0       1.0
      65.0       7.2
      66.0       1.1
      77.0       2.3
      78.0       1.1
      80.0       1.4
      91.0       1.3
      92.0       1.4
      93.0       2.0
      94.0       3.3
      95.0       1.0
     104.0       1.6
     120.0       1.0
     121.0       1.9
     122.0       5.2
     136.0       1.9
     148.0       6.2
     149.0       2.2
     150.0      21.2
     151.0       2.0
     162.0       1.8
     163.0       1.0
     164.0       2.4
     178.0     100.0
     179.0      11.6
     180.0       1.0
     192.0       4.2
     193.0      42.1
     194.0       5.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₅ N O₂	0.035 g : 0.5 ml CDCl₃
4-diethylamino-2-hydroxybenzaldehyde

    Assign.     Shift(ppm)

      A            11.6
      B             9.480
      C             7.259
      D             6.260
      E             6.064
      F             3.402
      G             1.206

     Hz     ppm     Int.

   4654.26  11.646    231
   3788.98   9.481    359
   2907.95   7.277     43
   2906.12   7.272    224
   2897.14   7.250    237
   2507.73   6.275    109
   2505.35   6.269    114
   2498.76   6.253    103
   2496.38   6.247    110
   2424.76   6.068    175
   2422.38   6.062    164
   1370.45   3.430    148
   1363.31   3.412    458
   1356.16   3.394    465
   1349.02   3.376    159
    489.05   1.224    520
    481.91   1.206   1000
    474.77   1.188    505

in CDCl3