P-ANISALDEHYDE DIMETHYL ACETAL(2186-92-7) ¹³C NMR

Product NameP-ANISALDEHYDE DIMETHYL ACETAL

CAS 2186-92-7

Molecular FormulaC10H14O3

Molecular Weight182.22

InChIInChI=1S/C10H14O3/c1-11-9-6-4-8(5-7-9)10(12-2)13-3/h4-7,10H,1-3H3

InChIKey NNHYAHOTXLASEA-UHFFFAOYSA-N

SmilesC1(C(OC)OC)=CC=C(OC)C=C1

Request For Quotation

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-5250          
p-anisaldehyde dimethyl acetal
C10H14O3            (Mass of molecular ion:    182)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.2
      28.0       1.1
      29.0       1.7
      31.0       1.4
      39.0       2.2
      50.0       1.2
      51.0       2.5
      59.0       1.0
      63.0       1.7
      64.0       1.8
      65.0       2.6
      75.0       3.4
      77.0       7.2
      78.0       1.9
      79.0       1.3
      91.0       3.0
      92.0       3.4
     107.0       3.6
     108.0       5.4
     121.0       1.9
     135.0      25.8
     136.0      15.4
     137.0       1.4
     151.0     100.0
     152.0      10.4
     182.0       6.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₄ O₃	0.05 ml : 0.5 ml CDCl₃
p-anisaldehyde dimethyl acetal

    Assign.     Shift(ppm)

      A             7.361
      B             6.883
      C             5.341
      D             3.779
      E             3.298

     Hz     ppm     Int.

   2946.47   7.373    122
   2944.79   7.369     43
   2939.76   7.356     45
   2938.08   7.352    140
   2758.33   6.902     21
   2755.43   6.895    159
   2753.45   6.890     53
   2748.72   6.878     50
   2746.58   6.873    153
   2135.01   5.343    150
   1510.62   3.780    622
   1318.21   3.299   1000

in CDCl3