TRIPHENYLMETHANESULFENYL CHLORIDE(24165-03-5) ¹H NMR

Product NameTRIPHENYLMETHANESULFENYL CHLORIDE

CAS 24165-03-5

Molecular FormulaC19H15ClS

Molecular Weight310.84

InChIInChI=1S/C19H15ClS/c20-21-19(16-10-4-1-5-11-16,17-12-6-2-7-13-17)18-14-8-3-9-15-18/h1-15H

InChIKey ZTQHJLXIUQQVST-UHFFFAOYSA-N

SmilesC(SCl)(C1C=CC=CC=1)(C1C=CC=CC=1)C1=CC=CC=C1

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Mass

MS-NW-9474          
triphenylmethanesulfenyl chloride
C19H15ClS           (Mass of molecular ion:    310)

   Source Temperature: 180 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      64.0       1.9
     113.0       1.1
     115.0       1.2
     119.5       2.0
     120.0       1.3
     139.0       1.2
     163.0       1.5
     164.0       1.8
     165.0      34.1
     166.0       5.8
     167.0       1.3
     202.0       2.0
     213.0       1.3
     215.0       4.4
     216.0       1.0
     226.0       3.1
     227.0       1.8
     228.0       7.7
     229.0       1.6
     237.0       1.6
     238.0       1.1
     239.0      12.1
     240.0       5.0
     241.0      20.8
     242.0      18.0
     243.0     100.0
     244.0      22.7
     245.0       2.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₉ H₁₅ Cl S	0.032 g : 0.5 ml CDCl₃
triphenylmethanesulfenyl chloride

    Assign.     Shift(ppm)

      A             7.35
      B             7.33
      C             7.31
     
     CONFIRMED BY LAOCN PROGRAM

     Hz     ppm     Int.

   2944.46   7.368     59
   2942.99   7.364     81
   2941.28   7.360    131
   2940.43   7.358    155
   2938.48   7.353    387
   2937.13   7.350    307
   2935.67   7.346    644
   2934.57   7.343    684
   2933.35   7.340    984
   2931.03   7.334    857
   2930.30   7.333   1000
   2927.61   7.326    469
   2926.03   7.322    363
   2924.32   7.318    500
   2922.97   7.314    263
   2922.00   7.312    271
   2920.53   7.308    161
   2919.07   7.305    182
   2914.67   7.294    116
   2911.99   7.287    124
   2906.86   7.274     30
   2900.76   7.259     32

in CDCl3