N-METHYLPYRROLE-2-ACETONITRILE(24437-41-0) ¹³C NMR

Product NameN-METHYLPYRROLE-2-ACETONITRILE

CAS 24437-41-0

Molecular FormulaC7H8N2

Molecular Weight120.15

Request For Quotation

Mass

MS-IW-1786          
1-methyl-2-pyrroleacetonitrile
C7H8N2              (Mass of molecular ion:    120)

   Source Temperature: 260 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       2.8
      26.0       1.1
      27.0       2.7
      28.0       2.8
      37.0       1.5
      38.0       2.7
      39.0       6.6
      40.0       1.6
      41.0       3.4
      42.0      10.8
      50.0       2.6
      51.0       6.2
      52.0       5.8
      53.0       4.6
      54.0       1.8
      63.0       2.3
      64.0       2.6
      65.0       8.2
      66.0       5.3
      67.0       2.9
      76.0       1.3
      77.0       1.4
      78.0       7.2
      79.0       3.2
      80.0       3.3
      91.0       1.8
      92.0      10.5
      93.0      20.9
      94.0      51.1
      95.0       3.5
     105.0       7.0
     118.0       4.3
     119.0      77.9
     120.0     100.0
     121.0       8.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₈ N₂	0.05 ml : 0.5 ml CDCl₃
1-methyl-2-pyrroleacetonitrile

    Assign.     Shift(ppm)

      A             6.612
      B             6.097
      C             6.053
      D             3.637
      E             3.578

     Hz     ppm     Int.

   2644.78   6.618    104
   2642.70   6.613    129
   2640.26   6.607    101
   2440.06   6.106     53
   2439.33   6.104     80
   2438.48   6.102     77
   2437.50   6.100     89
   2436.65   6.097     96
   2435.67   6.095    116
   2434.94   6.093    103
   2433.96   6.091    102
   2422.12   6.061    137
   2419.31   6.054    153
   2415.65   6.045     93
   1453.86   3.638    508
   1453.25   3.637    456
   1450.44   3.630     33
   1430.05   3.579   1000

in CDCl3