2,5-DICHLOROPHENYLHYDRAZINE(305-15-7) ¹³C NMR

Product Name2,5-DICHLOROPHENYLHYDRAZINE

CAS 305-15-7

Molecular FormulaC6H6Cl2N2

Molecular Weight177.03

InChIInChI=1S/C6H6Cl2N2/c7-4-1-2-5(8)6(3-4)10-9/h1-3,10H,9H2

InChIKey LZKWWERBNXLGLI-UHFFFAOYSA-N

SmilesN(C1=CC(Cl)=CC=C1Cl)N

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Mass

MS-IW-0722          
(2,5-dichlorophenyl)hydrazine
C6H6Cl2N2           (Mass of molecular ion:    176)

   Source Temperature: 250 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      17.0       1.7
      18.0       8.8
      28.0       5.5
      29.0       2.8
      31.0       5.5
      36.0       1.6
      37.0       1.7
      38.0       2.1
      39.0       1.1
      44.0       1.5
      44.5       1.0
      45.0       2.2
      49.0       1.3
      50.0       3.8
      51.0       3.6
      52.0       3.0
      61.0       2.3
      62.0       3.4
      63.0       5.6
      64.0       1.4
      73.0       5.5
      74.0       5.8
      75.0      13.0
      76.0       3.1
      77.0       7.2
      78.0       2.6
      83.0       1.0
      84.0       1.3
      85.0       2.1
      86.0       1.0
      87.0       1.2
      88.0       3.5
      89.0       2.2
      90.0       3.2
      97.0       2.5
      98.0       1.5
      99.0       2.2
     105.0       1.0
     109.0       3.7
     110.0       2.6
     111.0      19.4
     112.0       4.0
     113.0       6.3
     114.0       3.0
     124.0      15.0
     125.0       4.7
     126.0       6.3
     127.0       2.1
     133.0      35.1
     134.0       2.4
     135.0      22.3
     136.0       1.5
     137.0       3.6
     139.0       1.1
     141.0      25.9
     142.0       2.0
     143.0       8.3
     145.0       1.9
     146.0      17.9
     147.0       3.7
     148.0      11.6
     149.0       1.8
     150.0       2.1
     159.0       7.7
     160.0      30.1
     161.0      22.1
     162.0      20.5
     163.0      11.8
     164.0       4.0
     165.0       1.7
     174.0       1.1
     175.0       2.0
     176.0     100.0
     177.0       8.5
     178.0      63.6
     179.0       4.9
     180.0      10.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₆ Cl₂ N₂	0.037 g : 0.5 ml DMSO-d₆
(2,5-dichlorophenyl)hydrazine

    Assign.     Shift(ppm)

      A             7.198
      B             7.180
      C             6.86
      D             6.605
      E             4.3

     Hz     ppm     Int.

   2881.23   7.210    909
   2877.81   7.201     23
   2876.22   7.197     24
   2872.92   7.189   1000
   2870.85   7.184    719
   2868.29   7.178    717
   2861.33   7.160     21
   2741.46   6.860    429
   2645.02   6.619    545
   2642.46   6.612    529
   2639.65   6.605     28
   2636.60   6.598    495
   2634.03   6.591    493
   1721.07   4.307    149

in DMSO-d6