5-METHYL-2-NITROANISOLE(38512-82-2) ¹H NMR

Product Name5-METHYL-2-NITROANISOLE

CAS 38512-82-2

Molecular FormulaC8H9NO3

Molecular Weight167.16

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Mass

MS-NW-8941          
5-methyl-2-nitroanisole
C8H9NO3             (Mass of molecular ion:    167)

   Source Temperature: 250 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      18.0       1.0
      27.0       3.2
      28.0       3.3
      30.0       2.7
      31.0       1.6
      38.0       2.3
      39.0      15.6
      40.0       2.7
      41.0       4.7
      42.0       1.0
      43.0       2.4
      50.0       7.1
      51.0      16.6
      52.0      13.6
      53.0       6.5
      55.0       1.6
      62.0       3.1
      63.0      10.2
      64.0       3.7
      65.0      44.2
      66.0      11.3
      67.0       1.6
      74.0       1.5
      75.0       1.6
      76.0       2.8
      77.0      28.6
      78.0      28.2
      79.0      10.2
      80.0       1.3
      81.0       3.4
      89.0       9.4
      90.0       4.9
      91.0      64.3
      92.0      23.3
      93.0       6.8
      94.0       6.7
     105.0      20.0
     106.0      18.8
     107.0      11.8
     108.0       1.5
     109.0       9.5
     110.0       1.1
     119.0       1.8
     120.0     100.0
     121.0       8.3
     122.0       2.4
     137.0      32.0
     138.0       6.2
     150.0       1.1
     167.0      82.8
     168.0       8.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₉ N O₃	0.040 g : 0.5 ml CDCl₃
5-methyl-2-nitroanisole

    Assign.     Shift(ppm)

      A             7.780
      B             6.87
      C             6.82
      D             3.944
      E             2.419

     Hz     ppm     Int.

    701.31   7.831     97
    693.25   7.741    118
    615.19   6.870    172
    612.81   6.843     47
    607.00   6.778     62
    606.38   6.771     65
    605.38   6.760     53
    604.75   6.753     44
    353.25   3.945   1000
    216.75   2.421    590

in CDCl3