INDOLE-3-ACETIC ACID HYDRAZIDE(5448-47-5) ¹³C NMR

Product NameINDOLE-3-ACETIC ACID HYDRAZIDE

CAS 5448-47-5

Molecular FormulaC10H11N3O

Molecular Weight189.21

InChIInChI=1S/C10H11N3O/c11-13-10(14)5-7-6-12-9-4-2-1-3-8(7)9/h1-4,6,12H,5,11H2,(H,13,14)

InChIKey GYHLCXMCGCVVCG-UHFFFAOYSA-N

SmilesN1C2=C(C=CC=C2)C(CC(NN)=O)=C1

Request For Quotation

Mass

MS-NW-6678          
3-indoleacetohydrazide
C10H11N3O           (Mass of molecular ion:    189)

   Source Temperature: 200 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      18.0       3.8
      28.0       2.1
      31.0       3.1
      39.0       1.8
      50.0       2.7
      51.0       4.8
      52.0       2.3
      62.0       1.0
      63.0       2.5
      65.0       2.0
      74.0       2.0
      75.0       2.9
      76.0       3.6
      77.0      13.7
      78.0       1.7
     101.0       2.1
     102.0       7.0
     103.0      10.2
     104.0       1.3
     117.0       1.2
     128.0       4.1
     129.0       9.9
     130.0     100.0
     131.0      11.0
     144.0      17.6
     145.0       2.2
     146.0       1.0
     157.0       3.6
     158.0       3.4
     189.0      24.8
     190.0       3.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₁ N₃ O	0.039 g : 0.5 ml DMSO-d₆
3-indoleacetohydrazide

    Assign.     Shift(ppm)

      A            10.9
      B             9.15
      C             7.579
      D             7.338
      E             7.187
      F             7.062
      G             6.974
      J             4.21
      K             3.464

     Hz     ppm     Int.

   4343.61  10.869    146
   3658.20   9.154    201
   3033.42   7.591    217
   3033.05   7.590    219
   3025.54   7.571    237
   3025.18   7.570    232
   2937.07   7.350    272
   2928.83   7.329    319
   2873.52   7.191    316
   2871.32   7.185    306
   2831.02   7.084    117
   2829.92   7.081    127
   2824.06   7.067    191
   2822.96   7.064    253
   2821.86   7.061    134
   2816.00   7.047    161
   2814.72   7.043    150
   2794.94   6.994    178
   2794.20   6.992    176
   2787.06   6.974    271
   2786.33   6.972    198
   2780.10   6.957    124
   2779.00   6.954    114
   1683.67   4.213    413
   1384.56   3.465   1000

in DMSO-d6