2-(2-Chloroethyl)-N-methyl-pyrrolidine hydrochloride(56824-22-7) ¹³C NMR

Mass

MS-IW-0699          
2-(2-chloroethyl)-1-methylpyrrolidine hydrochloride
C7H14ClN HCl        (Mass of molecular ion:    147)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      27.0       1.0
      28.0       1.0
      36.0      15.5
      38.0       5.1
      41.0       2.1
      42.0      10.2
      55.0       1.4
      70.0       2.3
      82.0       4.6
      84.0     100.0
      85.0       6.0
     146.0       1.4
     147.0       4.2
     149.0       1.4

Assign. Shift(ppm) A 12.1 B 3.86 C 3.598 D 3.462 E 3.018 F 2.899 G 2.49 J 2.392 K 2.24 L 2.14 M 1.973 ASSIGNED BY H-H AND C-H COSY.

     Hz     ppm     Int.

   4839.44  12.110     35
   1558.93   3.901     35
   1553.98   3.889    129
   1550.69   3.881     54
   1548.67   3.876    197
   1545.38   3.867     83
   1542.45   3.860    181
   1539.88   3.854     85
   1537.13   3.847    237
   1534.20   3.839     78
   1532.00   3.834    108
   1528.71   3.826     39
   1450.31   3.629    106
   1445.00   3.616    111
   1441.89   3.608     87
   1441.52   3.607     87
   1438.77   3.601     94
   1436.39   3.595    117
   1433.46   3.587     92
   1430.35   3.580     72
   1429.80   3.578     69
   1424.85   3.566     87
   1395.55   3.492     41
   1388.04   3.474     66
   1379.98   3.453     68
   1372.47   3.435     44
   1223.92   3.063     37
   1216.41   3.044     71
   1215.13   3.041     59
   1212.56   3.035     42
   1207.62   3.022     82
   1205.05   3.016     74
   1203.77   3.013     55
   1200.11   3.003     47
   1197.54   2.997     53
   1196.26   2.994     70
   1188.75   2.975     38
   1161.09   2.906   1000
   1156.15   2.893    987
   1007.78   2.522     86
   1004.12   2.513     94
   1002.47   2.509    160
    998.99   2.500    170
    993.86   2.487    182
    989.83   2.477    149
    988.73   2.474     99
    984.52   2.464     84
    972.61   2.434     33
    968.22   2.423     35
    964.55   2.414     51
    959.98   2.403     81
    957.04   2.395     47
    955.40   2.391     49
    952.28   2.383     81
    947.15   2.370     57
    944.04   2.363     40
    939.46   2.351     43
    911.80   2.282     30
    906.49   2.269     45
    902.46   2.259     48
    898.43   2.249     76
    894.22   2.238     56
    892.94   2.235     40
    889.46   2.226     67
    884.88   2.215     51
    881.40   2.206     32
    873.52   2.186     33
    868.21   2.173     31
    864.91   2.165     52
    859.97   2.152     62
    857.22   2.145     59
    852.09   2.133     74
    848.61   2.124     38
    847.69   2.122     34
    846.60   2.119     31
    843.66   2.111     53
    838.72   2.099     31
    807.21   2.020     51
    799.70   2.002     48
    797.69   1.996     87
    794.21   1.988     48
    790.18   1.978     71
    788.17   1.973     55
    786.70   1.969     53
    784.69   1.964     75
    780.66   1.954     37
    777.18   1.945     62
    775.34   1.941     41