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Back ChemicalBook Home>CAS DataBase List>583-68-6More Spectrum> 2-Bromo-4-methylaniline(583-68-6) 1H NMR

2-Bromo-4-methylaniline(583-68-6) 1H NMR

Molecular FormulaC7H8BrN

Molecular Weight186.05

InChIInChI=1S/C7H8BrN/c1-5-2-3-7(9)6(8)4-5/h2-4H,9H2,1H3

InChIKey UVRRJILIXQAAFK-UHFFFAOYSA-N

SmilesC1(N)=CC=C(C)C=C1Br


  • Mass

    MS-NW-1580          
    2-bromo-p-toluidine
    C7H8BrN             (Mass of molecular ion:    185)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       1.2
          26.0       1.5
          27.0       4.9
          28.0       5.6
          30.0       2.2
          37.0       1.8
          38.0       3.5
          39.0       7.1
          39.5       1.4
          40.0       1.7
          41.0       2.0
          42.0       1.3
          49.0       1.2
          50.0       7.2
          51.0      16.2
          51.5       2.6
          52.0      15.5
          52.5      11.4
          53.0      15.4
          54.0       2.6
          61.0       1.4
          62.0       2.8
          63.0       4.8
          64.0       1.8
          65.0       3.0
          66.0       1.9
          74.0       1.7
          75.0       2.0
          76.0       3.2
          77.0      24.6
          78.0      15.9
          79.0      15.5
          80.0       2.6
          89.0       1.8
          91.0       1.2
          92.5       2.9
          93.5       2.6
         104.0      17.5
         105.0      13.3
         106.0      92.9
         107.0       9.1
         184.0      44.0
         185.0     100.0
         186.0      49.3
         187.0      96.5
         188.0       7.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H8 Br N 0.04 ml : 0.5 ml CDCl3
    2-bromo-p-toluidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.213 B 6.877 C 6.647 D 3.87 E 2.202

         Hz     ppm     Int.
    

        647.25   7.228    127
        646.56   7.220    179
        645.69   7.210    158
        645.31   7.206    149
        644.94   7.202    149
        622.56   6.952     71
        621.88   6.944     70
        621.25   6.937     46
        620.63   6.930     62
        620.00   6.923     57
        615.06   6.868     46
        614.50   6.862    127
        613.81   6.854    133
        613.19   6.847     88
        612.56   6.840    124
        611.88   6.833    120
        611.31   6.826     47
        598.00   6.678    315
        589.94   6.588    157
        346.69   3.872    509
        197.19   2.202   1000
    

in CDCl3



CCl4 solution



liquid film





2-Bromo-4-methylaniline(583-68-6) 1H NMR Atlas of Related Products

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