N-METHYL-P-TOLUIDINE(623-08-5) ¹³C NMR

Product NameN-METHYL-P-TOLUIDINE

CAS 623-08-5

Molecular FormulaC8H11N

Molecular Weight121.18

InChIInChI=1S/C8H11N/c1-7-3-5-8(9-2)6-4-7/h3-6,9H,1-2H3

InChIKey QCIFLGSATTWUQJ-UHFFFAOYSA-N

SmilesC1(NC)=CC=C(C)C=C1

Request For Quotation

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-6442          
N-methyl-p-toluidine
C8H11N              (Mass of molecular ion:    121)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       1.9
      28.0       1.5
      30.0       1.2
      38.0       1.0
      39.0       4.9
      41.0       1.5
      42.0       1.2
      50.0       2.2
      51.0       4.8
      52.0       3.4
      53.0       2.1
      58.5       2.4
      59.5       5.6
      60.0       1.9
      60.5       3.4
      62.0       1.3
      63.0       3.5
      64.0       1.2
      65.0       7.5
      66.0       1.2
      77.0       8.6
      78.0       4.3
      79.0       5.0
      80.0       1.4
      89.0       2.5
      90.0       1.8
      91.0      17.4
      92.0       4.7
      93.0       2.5
     104.0       2.5
     105.0       1.6
     106.0       8.3
     107.0       1.5
     118.0       4.0
     119.0       4.3
     120.0     100.0
     121.0      94.1
     122.0       8.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₁ N	0.05 ml : 0.5 ml CDCl₃
N-methyl-p-toluidine

    Assign.     Shift(ppm)

      A             7.032
      B             6.568
      C             3.46
      D             2.816
      E             2.279

     Hz     ppm     Int.

    634.31   7.083    183
    626.19   6.992    254
    591.44   6.604    293
    583.00   6.510    192
    309.81   3.460    262
    252.25   2.817   1000
    204.19   2.280    817

in CDCl3