p-cyanophenyl trans-4-pentylcyclohexanecarboxylate(62439-35-4) ¹³C NMR

Mass

MS-NW-4499          
p-cyanophenyl trans-4-pentylcyclohexanecarboxylate
C19H25NO2           (Mass of molecular ion:    299)

   Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       2.8
      27.0       6.7
      28.0       1.2
      29.0      12.2
      39.0       8.0
      40.0       1.4
      41.0      31.6
      42.0       2.4
      43.0      19.5
      51.0       1.1
      53.0       5.3
      54.0       9.2
      55.0      48.9
      56.0       3.3
      57.0      18.0
      63.0       1.7
      64.0       2.2
      65.0       1.5
      66.0       1.1
      67.0      20.9
      68.0       4.5
      69.0      40.0
      70.0       2.6
      71.0      22.5
      72.0       1.3
      77.0       1.6
      79.0       3.7
      80.0       1.3
      81.0      22.2
      82.0       5.6
      83.0      87.5
      84.0       6.0
      85.0       5.1
      90.0       3.7
      91.0       1.7
      95.0       8.5
      96.0       3.5
      97.0     100.0
      98.0       7.6
     102.0       2.1
     109.0       2.9
     111.0      25.5
     112.0       2.4
     118.0       1.4
     119.0       3.7
     120.0       2.0
     151.0       1.0
     153.0      60.1
     154.0       7.7
     181.0      61.5
     182.0       8.5

Assign. Shift(ppm) A 7.678 B 7.209 C 2.491 D 2.126 E 1.886 F 1.542 G 1.37 to 1.19 J 1.21 K 0.982 L 0.890

     Hz     ppm     Int.

   3075.20   7.695    114
   3072.75   7.689    759
   3070.68   7.684    240
   3067.87   7.677     39
   3066.04   7.672    255
   3063.84   7.667    812
   3061.52   7.661    114
   2887.45   7.225    124
   2885.13   7.220    835
   2883.06   7.214    248
   2880.62   7.208     40
   2878.30   7.203    246
   2876.22   7.197    738
   2873.78   7.191    101
   1011.60   2.532     37
   1008.06   2.523     77
   1004.52   2.514     47
    999.39   2.501     82
    995.85   2.492    162
    992.31   2.483     87
    987.18   2.471     49
    983.64   2.462     86
    979.98   2.453     43
    858.03   2.147    122
    856.57   2.144    120
    854.74   2.139    125
    854.49   2.139    125
    853.27   2.136    104
    849.49   2.126     70
    844.36   2.113    137
    843.87   2.112    135
    842.29   2.108    126
    840.94   2.105    130
    760.74   1.904    127
    760.01   1.902    126
    759.77   1.902    126
    758.18   1.898    136
    753.05   1.885     58
    747.44   1.871    137
    747.19   1.870    137
    744.26   1.863    130
    636.96   1.594     61
    633.42   1.585     57
    623.78   1.561    161
    620.24   1.552    144
    611.45   1.530    149
    607.79   1.521    142
    598.14   1.497     57
    594.73   1.489     51
    540.41   1.353     41
    539.43   1.350     36
    537.35   1.345     57
    537.11   1.344     57
    533.20   1.335    116
    530.88   1.329    114
    526.86   1.319    216
    525.63   1.316    222
    520.39   1.303    293
    519.17   1.300    286
    518.68   1.298    285
    513.55   1.285    303
    512.45   1.283    306
    509.64   1.276    289
    507.69   1.271    285
    505.74   1.266    240
    504.03   1.262    245
    499.88   1.251    176
    497.44   1.245    183
    491.82   1.231    219
    489.62   1.226    192
    487.30   1.220    175
    485.11   1.214    179
    478.15   1.197    115
    472.41   1.183     45
    470.21   1.177     34
    469.97   1.176     34
    412.23   1.032     67
    408.94   1.024     68
    399.05   0.999    148
    395.63   0.990    126
    392.09   0.982     30
    387.82   0.971    111
    384.77   0.963    121
    374.39   0.937     60
    371.22   0.929     58
    369.02   0.924     34
    367.19   0.919     48
    363.04   0.909    344
    356.08   0.891   1000
    353.64   0.885     86
    348.88   0.873    390