3-Methylphenylhydrazine hydrochloride(637-04-7) ¹³C NMR

Product Name3-Methylphenylhydrazine hydrochloride

CAS 637-04-7

Molecular FormulaC7H11ClN2

Molecular Weight158.63

InChIInChI=1S/C7H10N2.ClH/c1-6-3-2-4-7(5-6)9-8;/h2-5,9H,8H2,1H3;1H

InChIKey SHTBTGXNVWYODU-UHFFFAOYSA-N

SmilesN(C1=CC=CC(C)=C1)N.[H]Cl

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Mass

MS-NW-0640          
m-tolylhydrazine hydrochloride
C7H10N2 HCl         (Mass of molecular ion:    122)

   Source Temperature: 190 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      18.0       1.2
      27.0       3.3
      28.0       2.7
      29.0       2.3
      31.0       1.3
      35.0       3.9
      36.0      29.4
      37.0       1.3
      38.0       9.6
      39.0      10.8
      40.0       1.3
      41.0       2.7
      50.0       3.7
      51.0       8.0
      52.0       4.8
      53.0       3.4
      60.0       1.9
      61.0       1.9
      62.0       1.9
      63.0       5.2
      64.0       2.1
      65.0      11.4
      66.0       1.7
      67.0       1.1
      76.0       1.2
      77.0      29.5
      78.0      13.8
      79.0      33.2
      80.0       3.7
      89.0       2.6
      90.0       1.3
      91.0      21.3
      92.0      12.7
      93.0       4.9
      94.0       2.5
     104.0      10.3
     105.0       5.4
     106.0      34.6
     107.0      10.0
     121.0       4.4
     122.0     100.0
     123.0       8.4

90 MHz in D2O

¹H NMR	89.56 MHz
C₇ H₁₀ N₂	saturated in D₂O
m-tolylhydrazine hydrochloride

    Assign.     Shift(ppm)

      A             7.32
      B             7.01
      C             6.92
      D             6.90
      E             2.346
     
     SOLVENT PEAK REMOVED

     Hz     ppm     Int.

    664.94   7.425     60
    657.50   7.342    116
    650.38   7.262     79
    648.63   7.243    139
    631.19   7.048    158
    620.00   6.923    382
    613.19   6.847    102
    210.25   2.348   1000

in D2O