4-Methyl-3-nitrobenzyl chloride(84540-59-0) ¹³C NMR

Mass

MS-NW-7904          
4-methyl-3-nitrobenzyl chloride
C8H8ClNO2           (Mass of molecular ion:    185)

   Source Temperature: 140 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      18.0       1.6
      26.0       1.1
      27.0       6.8
      28.0       2.7
      30.0       2.9
      37.0       1.0
      38.0       2.9
      39.0      12.5
      40.0       1.1
      41.0       1.5
      49.0       1.3
      50.0       9.4
      51.0      23.2
      52.0       6.4
      53.0       4.5
      61.0       1.5
      62.0       4.1
      63.0      11.4
      64.0       2.2
      65.0       6.5
      66.0       1.3
      66.5       1.6
      67.0       1.0
      68.0       1.8
      73.0       2.1
      74.0       3.1
      75.0       6.8
      76.0       4.2
      77.0      75.7
      78.0      23.3
      79.0       2.6
      86.0       1.0
      87.0       1.5
      89.0       4.5
      90.0       1.5
      91.0      13.1
      92.0       4.8
      99.0       1.3
     101.0       3.1
     102.0       9.9
     103.0      53.8
     104.0      47.3
     105.0      12.2
     106.0       3.0
     113.0      11.3
     114.0       1.1
     115.0       3.5
     120.0       3.6
     121.0       1.5
     132.0      15.7
     133.0       9.4
     134.0       1.1
     138.0       1.9
     139.0       6.6
     140.0       6.1
     141.0       2.6
     142.0       1.7
     150.0      15.9
     151.0       1.4
     168.0     100.0
     169.0       9.7
     170.0      36.3
     171.0       3.2
     185.0      27.5
     186.0       2.8
     187.0       8.6
     188.0       1.0

Assign. Shift(ppm) A 7.996 B 7.526 C 7.357 D 4.604 E 2.595

     Hz     ppm     Int.

    717.13   8.008    184
    715.25   7.987    182
    680.44   7.598     71
    678.50   7.576     61
    672.56   7.510    159
    670.63   7.489    144
    661.31   7.384    205
    653.31   7.295     88
    412.44   4.606    694
    232.44   2.596   1000