1004-66-6

2,6-二甲基大茴香醚(1004-66-6)Raman光谱

产品名称:2,6-二甲基大茴香醚

CAS:1004-66-6

分子式:C9H12O

分子量: 136.19

InChI:InChI=1S/C9H12O/c1-7-5-4-6-8(2)9(7)10-3/h4-6H,1-3H3

InChIKey: GFNZJAUVJCGWLW-UHFFFAOYSA-N

Smiles:C1(C)=CC=CC(C)=C1OC

¹HNMR

IR1

Raman

Mass

MS-NW-5644          
2,6-dimethylanisole
C9H12O              (Mass of molecular ion:    136)

   Source Temperature: 280 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.9
      27.0       5.2
      38.0       1.3
      39.0       9.5
      40.0       1.3
      41.0       3.8
      43.0       1.4
      50.0       2.8
      51.0       7.6
      52.0       3.2
      53.0       5.3
      62.0       1.5
      63.0       4.1
      64.0       1.1
      65.0       7.8
      66.0       1.1
      77.0      34.5
      78.0       9.2
      79.0       4.8
      89.0       1.2
      91.0      33.4
      92.0       4.2
      93.0       9.4
     103.0       6.4
     104.0       5.3
     105.0      13.1
     106.0       2.4
     107.0       1.1
     121.0      84.6
     122.0       9.4
     135.0       3.8
     136.0     100.0
     137.0      10.1

90 MHz in CDCl3

400 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₂ O	0.04 ml : 0.5 ml CDCl₃
2,6-dimethylanisole

    Assign.     Shift(ppm)

      A             7.00
      B             6.90
      C             3.707
      D             2.277

     Hz     ppm     Int.

    628.31   7.016     25
    624.38   6.972    125
    623.94   6.967    131
    622.00   6.946    179
    618.06   6.902     28
    332.06   3.708   1000
    330.19   3.687     21
    203.94   2.278    725

¹H NMR	399.65 MHz
C₉ H₁₂ O	0.05 ml : 0.5 ml CDCl₃
2,6-dimethylanisole

    Assign.     Shift(ppm)

      A             6.975
      B             6.889
      C             3.684
      D             2.269
     
     90MHZ. : HSP-03-275

     Hz     ppm     Int.

   2792.48   6.988    137
   2791.75   6.986    137
   2791.14   6.984    104
   2785.77   6.971    158
   2785.16   6.969    224
   2784.55   6.968    229
   2783.94   6.966    173
   2759.52   6.905    122
   2752.93   6.889     88
   2751.34   6.885     83
   2744.63   6.868     56
   1472.41   3.685   1000
    907.23   2.271    815
    906.49   2.269    854

liquid film