101930-07-8

(R)-(+)-N-苄基-3-羟基吡咯烷(101930-07-8)质谱(MS)

产品名称:(R)-(+)-N-苄基-3-羟基吡咯烷

CAS:101930-07-8

分子式:C11H15NO

分子量: 177.24

InChI:InChI=1S/C11H15NO/c13-11-6-7-12(9-11)8-10-4-2-1-3-5-10/h1-5,11,13H,6-9H2/t11-/m1/s1

InChIKey: YQMXOIAIYXXXEE-LLVKDONJSA-N

Smiles:N1(CC2=CC=CC=C2)CC[C@@H](O)C1

¹HNMR

IR1

Raman

Mass

MS-IW-4097          
(R)-1-benzyl-3-pyrrolidinol
C11H15NO            (Mass of molecular ion:    177)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.0
      27.0       1.4
      28.0       2.3
      29.0       1.5
      30.0       1.8
      39.0       4.1
      41.0       4.7
      42.0      86.4
      43.0       5.6
      44.0       3.5
      51.0       2.5
      55.0       2.2
      56.0       1.2
      57.0       2.1
      58.0       1.3
      63.0       2.2
      65.0      17.3
      66.0       1.1
      68.0       1.2
      70.0       1.4
      77.0       2.4
      82.0       1.1
      86.0      36.6
      87.0       1.8
      89.0       3.4
      90.0       1.8
      91.0     100.0
      92.0      13.5
     100.0      23.9
     101.0       1.5
     104.0       4.1
     105.0       2.4
     118.0       2.6
     120.0       2.2
     131.0       1.1
     132.0      27.1
     133.0      37.1
     134.0       4.3
     157.0       2.0
     158.0       1.2
     176.0      17.5
     177.0      43.4
     178.0       5.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₅ N O	0.05 ml : 0.5 ml CDCl₃
(R)-1-benzyl-3-pyrrolidinol

    Assign.     Shift(ppm)

      A             7.28
      B             7.24
      C             4.273
      D             4.05
      E             3.579
      F     *1      2.779
      G             2.575
      J             2.558
      K     *2      2.316
      L     *1      2.131
      M     *2      1.679

     Hz     ppm     Int.

   2918.70   7.304     66
   2914.55   7.293    796
   2914.06   7.292    762
   2910.40   7.283    730
   2909.67   7.281    780
   2904.05   7.267     74
   2902.10   7.262     80
   2900.76   7.259     85
   2899.66   7.256     71
   2896.36   7.248    187
   2895.75   7.246    131
   2892.46   7.238    112
   2891.48   7.236    136
   2889.65   7.231     77
   2888.43   7.228     71
   2887.21   7.225    141
   2884.89   7.219     60
   2884.16   7.217     50
   2882.81   7.214     74
   2881.35   7.210     43
   2878.42   7.203     31
   1717.29   4.297     43
   1714.23   4.290     76
   1712.04   4.284     66
   1711.18   4.282     71
   1709.59   4.278    108
   1706.54   4.271    107
   1704.47   4.265     72
   1703.74   4.264     66
   1701.66   4.258     79
   1698.61   4.251     46
   1620.48   4.055     42
   1430.42   3.580   1000
   1121.58   2.807     61
   1116.21   2.793     72
   1113.28   2.786     99
   1112.43   2.784     90
   1107.91   2.773     99
   1107.06   2.771     99
   1104.13   2.763     84
   1098.88   2.750     77
   1034.79   2.590     37
   1027.71   2.572    283
   1026.25   2.568    384
   1024.66   2.564    243
   1021.12   2.556    298
   1015.99   2.543     47
   1010.99   2.530     54
    938.72   2.349     71
    932.25   2.333     94
    930.18   2.328    122
    923.71   2.312    126
    923.10   2.310    117
    921.02   2.305     94
    914.55   2.289     88
    868.41   2.173     44
    863.16   2.160     49
    860.84   2.154     56
    860.11   2.153     54
    854.86   2.140     99
    852.42   2.133     48
    849.49   2.126     64
    847.17   2.120     98
    841.80   2.107     67
    838.87   2.100     47
    833.50   2.086     39
    685.79   1.716     38
    683.23   1.710     37
    679.20   1.700     47
    677.49   1.696     61
    675.29   1.690     49
    671.75   1.681     58
    669.07   1.675     58
    665.65   1.666     45
    663.45   1.661     53
    661.62   1.656     42
    657.71   1.646     35
    655.03   1.640     32

liquid film