138-89-6

N,N-二甲基-4-亚硝基苯胺(138-89-6)红外图谱(IR2)

产品名称:N,N-二甲基-4-亚硝基苯胺

CAS:138-89-6

分子式:C8H10N2O

分子量: 150.18

InChI:InChI=1S/C8H10N2O/c1-10(2)8-5-3-7(9-11)4-6-8/h3-6H,1-2H3

InChIKey: CMEWLCATCRTSGF-UHFFFAOYSA-N

Smiles:C1(N(C)C)=CC=C(N=O)C=C1

Mass

MS-NW-4763          
N,N-dimethyl-p-nitrosoaniline
C8H10N2O            (Mass of molecular ion:    150)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       4.6
      17.0       1.1
      18.0       5.5
      27.0       2.0
      28.0       2.0
      29.0       1.7
      30.0       3.3
      37.0       1.6
      38.0       2.9
      39.0       6.6
      40.0       1.2
      41.0       2.4
      42.0      36.0
      43.0       2.3
      44.0       4.2
      50.0       8.4
      51.0       8.4
      52.0       4.7
      53.0       2.3
      54.0       1.1
      61.0       1.0
      62.0       2.0
      63.0       8.6
      64.0       3.9
      65.0       7.0
      66.0       4.0
      67.0       1.3
      68.0       2.6
      69.0       1.7
      74.0       3.1
      75.0       2.9
      76.0       6.5
      77.0      35.7
      78.0      15.8
      79.0      20.2
      80.0       3.8
      81.0       1.4
      90.0       6.4
      91.0      17.2
      92.0      10.7
      93.0       5.8
      94.0       2.4
     102.0       1.0
     103.0       3.5
     104.0      22.3
     105.0      37.1
     106.0       3.8
     107.0       1.0
     117.0       2.3
     118.0      13.7
     119.0      26.4
     120.0      37.4
     121.0       5.2
     132.0       1.6
     133.0       2.5
     134.0       2.1
     135.0       2.1
     136.0       3.7
     147.0       2.1
     148.0       2.7
     150.0     100.0
     151.0      10.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₀ N₂ O	0.029 g : 0.5 ml CDCl₃
N,N-dimethyl-p-nitrosoaniline

    Assign.     Shift(ppm)

      A             7.79
      B             6.654
      C             3.138
     
     90MHZ : HSP-06-120 AT ROOM TEMP

     Hz     ppm     Int.

    702.69   7.847     27
    702.31   7.842     27
    701.63   7.835     26
    694.13   7.751     30
    693.50   7.744     31
    600.19   6.702     83
    599.00   6.689     42
    592.13   6.612     39
    590.75   6.597     68
    281.06   3.139   1000

in CDCl3