2-哌啶乙醇(1484-84-0)红外图谱(IR2)
InChI:InChI=1S/C7H15NO/c9-6-4-7-3-1-2-5-8-7/h7-9H,1-6H2
InChIKey: PTHDBHDZSMGHKF-UHFFFAOYSA-N
Smiles:N1CCCCC1CCO
-
Mass
MS-NW-9203
2-piperidineethanol
C7H15NO (Mass of molecular ion: 129)
Source Temperature: 250 °C
Sample Temperature: 150 °C
Reservoir, 75 eV
18.0 4.8
27.0 3.1
28.0 7.3
29.0 3.0
30.0 9.3
31.0 2.4
39.0 2.8
41.0 6.1
42.0 6.9
43.0 4.5
44.0 4.5
45.0 1.1
53.0 1.2
54.0 2.8
55.0 6.8
56.0 14.8
57.0 2.6
67.0 1.7
68.0 1.7
69.0 1.0
70.0 2.8
72.0 4.0
82.0 2.5
83.0 1.2
84.0 100.0
85.0 6.2
86.0 1.0
98.0 4.6
100.0 1.0
110.0 1.3
111.0 1.0
128.0 1.6
129.0 1.4
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C7 H15 N O
|
0.040 g : 0.5 ml CDCl3
|
| 2-piperidineethanol
|
 |
Assign. Shift(ppm)
A *1 3.77
B *1 3.75
C 3.32
D 3.02
E 2.74
F 2.60
G 1.84 to 1.19
J 1.59
|
Hz ppm Int.
348.44 3.891 35
343.06 3.831 418
342.38 3.823 401
341.13 3.809 88
340.50 3.802 82
337.00 3.763 895
332.19 3.710 377
330.69 3.693 408
327.94 3.662 32
325.44 3.634 34
319.75 3.571 36
297.63 3.324 1000
282.69 3.157 30
280.38 3.131 68
279.06 3.116 83
277.31 3.097 90
275.00 3.071 55
269.94 3.015 61
267.13 2.983 165
266.75 2.979 165
264.50 2.954 180
257.50 2.876 51
255.31 2.851 39
254.75 2.845 40
251.44 2.808 95
248.50 2.775 85
248.19 2.772 85
247.38 2.763 94
245.19 2.738 179
242.00 2.703 178
239.50 2.675 119
235.13 2.626 147
234.00 2.613 170
232.56 2.597 145
229.56 2.564 62
229.19 2.560 62
226.38 2.528 34
225.13 2.514 37
221.56 2.474 71
220.13 2.458 48
218.56 2.441 57
170.69 1.906 32
169.44 1.892 49
167.81 1.874 63
166.56 1.860 82
163.31 1.824 101
161.69 1.806 136
160.00 1.787 132
157.81 1.763 123
155.00 1.731 85
153.06 1.710 139
149.25 1.667 534
147.13 1.643 218
146.44 1.636 235
143.75 1.606 784
140.44 1.569 329
137.94 1.541 870
136.56 1.525 480
134.56 1.503 334
132.56 1.481 370
131.44 1.468 331
126.69 1.415 219
125.75 1.405 195
125.19 1.398 193
124.19 1.387 174
120.31 1.344 225
118.63 1.325 238
117.50 1.312 207
116.06 1.296 172
113.19 1.264 102
111.00 1.240 128
106.25 1.187 70
102.81 1.148 31
102.38 1.144 33
101.94 1.139 34
100.75 1.125 46
100.31 1.121 43
100.00 1.117 42
96.75 1.081 57
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| 1H NMR |
399.65 MHz |
| C7 H15 N O
|
0.034 g : 0.5 ml CDCl3
|
| 2-piperidineethanol
|
|
Assign. Shift(ppm)
A *1 3.80
B *1 3.75
C 3.2
D 3.032
E 2.740
F 2.597
G 1.810
J 1.61
K 1.57
L *2 1.42
M *2 1.35
N 1.35
ASSIGNED BY H-H COSY.
90MHZ : HSP-03-798
|
Hz ppm Int.
1532.35 3.835 170
1527.22 3.822 299
1521.48 3.808 478
1516.36 3.795 791
1511.35 3.782 428
1509.03 3.776 454
1503.91 3.764 276
1503.05 3.761 331
1502.44 3.760 425
1502.08 3.759 418
1498.17 3.749 216
1496.70 3.746 465
1493.16 3.737 115
1492.43 3.735 130
1491.09 3.731 178
1485.84 3.718 193
1222.17 3.059 137
1220.09 3.053 196
1218.14 3.049 233
1215.94 3.043 205
1213.87 3.038 137
1209.47 3.027 154
1207.40 3.022 202
1205.44 3.017 279
1203.86 3.013 241
1201.42 3.007 134
1107.79 2.772 109
1105.10 2.766 121
1100.59 2.754 168
1098.39 2.749 146
1096.68 2.745 178
1094.12 2.738 179
1093.26 2.736 172
1089.72 2.727 173
1087.40 2.721 136
1084.84 2.715 131
1082.15 2.708 122
1051.15 2.631 252
1048.34 2.624 235
1038.82 2.600 370
1036.50 2.594 276
1035.77 2.592 285
1026.61 2.569 243
1023.93 2.563 178
732.30 1.833 118
730.35 1.828 151
728.76 1.824 166
727.17 1.820 134
725.22 1.815 130
723.88 1.812 105
721.19 1.805 139
719.12 1.800 145
717.77 1.796 195
715.94 1.792 206
713.01 1.785 132
655.52 1.641 210
652.83 1.634 210
650.63 1.628 122
649.05 1.625 124
645.51 1.616 285
642.70 1.609 439
641.48 1.606 399
640.87 1.604 409
639.89 1.602 409
636.96 1.594 689
631.59 1.581 1000
630.49 1.578 945
625.61 1.566 955
623.17 1.560 369
621.09 1.555 291
618.29 1.548 255
582.15 1.457 181
578.61 1.448 279
574.95 1.439 133
569.46 1.425 206
565.92 1.417 331
562.74 1.409 184
556.88 1.394 136
555.42 1.390 129
554.81 1.389 126
552.98 1.384 246
550.42 1.378 152
548.46 1.373 123
543.33 1.360 173
539.79 1.351 273
535.89 1.341 154
531.37 1.330 124
527.47 1.320 216
523.80 1.311 125
498.29 1.247 125
494.63 1.238 150
487.43 1.220 151
485.72 1.216 204
483.76 1.211 189
481.93 1.206 203
474.61 1.188 172
473.27 1.185 137
470.83 1.179 187