1514-26-7

间(4-氟苯氧基)甲苯(1514-26-7)质谱(MS)

产品名称:间(4-氟苯氧基)甲苯

CAS:1514-26-7

分子式:C13H11FO

分子量: 202.22

InChI:InChI=1S/C13H11FO/c1-10-3-2-4-13(9-10)15-12-7-5-11(14)6-8-12/h2-9H,1H3

InChIKey: APVQRVSBMIDSFS-UHFFFAOYSA-N

Smiles:C1(OC2=CC=C(F)C=C2)=CC=CC(C)=C1

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9285          
m-(p-fluorophenoxy)toluene
C13H11FO            (Mass of molecular ion:    202)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       1.8
      38.0       1.2
      39.0      10.5
      41.0       3.4
      50.0       2.9
      51.0       6.0
      52.0       1.7
      53.0       1.4
      57.0       2.5
      62.0       1.5
      63.0       6.3
      64.0       2.1
      65.0      26.7
      66.0       1.5
      69.0       1.3
      74.0       1.2
      75.0       4.7
      76.0       2.2
      77.0       3.5
      78.0       5.9
      79.0       1.9
      83.0       2.6
      85.0       1.4
      86.0       1.0
      89.0       5.7
      90.0       3.1
      91.0      40.5
      92.0       3.3
      95.0       2.2
      96.0       1.0
      99.5       1.2
     100.0       8.6
     100.5       1.3
     101.0       1.7
     107.0       1.5
     109.0       7.1
     112.0       1.6
     115.0       1.5
     133.0       4.3
     146.0       2.9
     147.0       1.9
     152.0       1.8
     153.0       3.4
     159.0      16.8
     160.0       2.2
     170.0       1.0
     171.0       1.1
     173.0       8.9
     174.0       9.4
     175.0       1.2
     183.0       1.4
     186.0       2.7
     187.0       5.8
     198.0       1.2
     199.0       1.4
     201.0       5.9
     202.0     100.0
     203.0      14.2
     204.0       1.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₁ F O	0.05 ml : 0.5 ml CDCl₃
m-(p-fluorophenoxy)toluene

    Assign.     Shift(ppm)

      A             7.173
      B             6.99
      C             6.95
      D             6.880
      E             6.777
      F             6.747
      G             2.297

     Hz     ppm     Int.

   2875.12   7.195    133
   2867.31   7.175    256
   2859.50   7.156    162
   2800.90   7.009    148
   2798.10   7.002     71
   2794.07   6.992    144
   2793.09   6.989    165
   2791.50   6.985    409
   2788.33   6.977     85
   2786.38   6.973    124
   2783.69   6.966    447
   2780.76   6.958    447
   2778.69   6.953    124
   2778.08   6.952    131
   2776.12   6.947    398
   2774.05   6.942    105
   2773.32   6.940    124
   2771.36   6.935    150
   2769.53   6.930     71
   2768.31   6.927     40
   2766.60   6.923    110
   2754.52   6.893    137
   2753.66   6.891    150
   2752.93   6.889    133
   2746.95   6.874    119
   2746.09   6.872    133
   2745.36   6.870    119
   2708.74   6.778    211
   2702.15   6.762    142
   2699.71   6.756     91
   2694.09   6.742    115
   2691.65   6.736     92
    918.21   2.298   1000

in CDCl3