1581-13-1

2-氨基-2'-氟苯甲酮(1581-13-1)红外图谱(IR1)

产品名称:2-氨基-2'-氟苯甲酮

CAS:1581-13-1

分子式:C13H10FNO

分子量: 215.22

Mass

MS-IW-0787          
2-amino-2'-fluorobenzophenone
C13H10FNO           (Mass of molecular ion:    215)

   Source Temperature: 140 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      28.0       1.0
      39.0       3.7
      51.0       1.0
      52.0       1.2
      63.0       1.9
      64.0       1.8
      65.0      15.2
      66.0       1.7
      75.0       4.4
      83.5       3.5
      85.0       1.0
      91.0       1.3
      92.0      22.2
      92.5       1.7
      93.0       2.1
      95.0      12.6
      96.0       1.0
     107.0       1.1
     107.5       3.8
     119.0       2.2
     120.0      39.7
     121.0       3.3
     123.0      15.2
     124.0       1.2
     139.0       1.6
     166.0       3.1
     167.0       3.9
     168.0       1.1
     185.0       3.0
     186.0       6.6
     187.0       1.2
     194.0       2.9
     195.0      10.2
     196.0      17.7
     197.0       2.8
     198.0      11.2
     199.0       1.6
     214.0      69.6
     215.0     100.0
     216.0      14.2
     217.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₀ F N O	0.038 g : 0.5 ml CDCl₃
2-amino-2'-fluorobenzophenone

    Assign.     Shift(ppm)

      A             7.455
      B             7.409
      C             7.314
      D             7.325
      E             7.228
      F             7.142
      G             6.703
      J             6.568
      K             6.39

     Hz     ppm     Int.

   2989.75   7.481    199
   2987.92   7.477    233
   2984.50   7.468    217
   2982.67   7.464    414
   2981.45   7.461    299
   2980.59   7.459    340
   2979.61   7.456    310
   2977.17   7.450    290
   2976.20   7.448    297
   2975.34   7.445    359
   2974.37   7.443    461
   2972.29   7.438    337
   2968.38   7.428    468
   2966.92   7.424    497
   2960.82   7.409    601
   2959.72   7.406    485
   2959.35   7.405    481
   2953.98   7.392    483
   2952.15   7.387    388
   2931.15   7.335    305
   2929.32   7.330    454
   2927.37   7.325    372
   2922.97   7.314    335
   2921.26   7.310    507
   2919.56   7.306    762
   2918.09   7.302    436
   2915.53   7.296     59
   2912.60   7.288    532
   2911.25   7.285    728
   2909.79   7.281    431
   2906.98   7.274     52
   2904.30   7.268    488
   2902.71   7.264    410
   2900.02   7.257     46
   2896.12   7.247    626
   2895.02   7.244    664
   2892.58   7.238     49
   2891.60   7.236     53
   2888.67   7.229    962
   2887.57   7.226    978
   2884.64   7.218     51
   2884.03   7.217     45
   2881.10   7.210    455
   2880.00   7.207    460
   2863.40   7.165    452
   2862.30   7.163    436
   2854.74   7.144    456
   2853.76   7.141    757
   2852.66   7.138    477
   2845.34   7.120    400
   2844.36   7.118    390
   2683.72   6.716    760
   2683.23   6.714    794
   2682.62   6.713    820
   2679.81   6.706     45
   2675.29   6.695    726
   2674.93   6.694    751
   2674.19   6.692    756
   2632.81   6.588    566
   2631.71   6.586    538
   2629.52   6.580     40
   2629.03   6.579     40
   2625.73   6.571    606
   2624.76   6.568   1000
   2623.66   6.565    542
   2621.46   6.560     49
   2621.09   6.559     48
   2620.36   6.557     43
   2619.75   6.556     42
   2617.68   6.550    532
   2616.58   6.548    486
   2552.25   6.387    357

in CDCl3