20082-71-7

五氟苯基二甲基氯硅烷(20082-71-7)红外图谱(IR1)

产品名称:五氟苯基二甲基氯硅烷

CAS:20082-71-7

分子式:C8H6ClF5Si

分子量: 260.66

InChI:InChI=1S/C8H6ClF5Si/c1-15(2,9)8-6(13)4(11)3(10)5(12)7(8)14/h1-2H3

InChIKey: PQRFRTCWNCVQHI-UHFFFAOYSA-N

Smiles:C1([Si](Cl)(C)C)=C(F)C(F)=C(F)C(F)=C1F

¹HNMR

IR1

Mass

MS-IW-2071          
chlorodimethyl(pentafluorophenyl)silane
C8H6ClF5Si          (Mass of molecular ion:    260)

   Source Temperature: 200 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       2.9
      27.0       2.7
      28.0       2.9
      29.0       1.9
      31.0       5.7
      39.0       1.5
      42.0       1.3
      43.0       2.3
      47.0      31.2
      48.0       1.8
      49.0       7.0
      50.0       1.5
      51.0       7.0
      57.0       5.5
      61.0       3.3
      62.0       2.3
      63.0      14.3
      64.0       1.3
      65.0       8.7
      67.0       5.6
      68.0       1.5
      69.0       4.8
      73.0       3.3
      74.0       4.4
      75.0      29.1
      76.0       3.3
      77.0      26.2
      78.0       3.3
      79.0      16.3
      80.0       5.4
      81.0      45.6
      82.0       3.2
      83.0       5.6
      85.0       7.4
      86.0       2.3
      87.0       2.2
      91.0       9.7
      92.0       4.9
      93.0      25.6
      94.0       3.1
      95.0       8.9
      96.0       4.5
      97.0      59.6
      98.0      10.8
      99.0      30.1
     100.0       2.1
     101.0       8.4
     102.0       1.1
     103.0       2.4
     104.0       1.8
     105.0       6.0
     106.0       5.5
     107.0       2.2
     109.0       2.6
     110.0       9.5
     111.0       8.1
     112.0       1.7
     113.0       2.4
     114.0       1.3
     115.0       4.2
     117.0       6.7
     119.0       7.4
     122.5      11.6
     123.0       6.3
     123.5       4.3
     124.0       1.7
     125.0      54.1
     126.0       5.2
     127.0       1.5
     129.0      26.4
     130.0       3.1
     133.0       1.6
     135.0      20.8
     136.0       1.2
     137.0       8.3
     138.0       1.3
     139.0       2.5
     141.0      25.4
     142.0       2.6
     143.0      18.0
     144.0       5.2
     145.0      24.6
     146.0       2.6
     147.0       8.0
     148.0       5.8
     155.0       9.2
     156.0       1.7
     157.0       3.8
     158.0       2.1
     159.0      15.1
     160.0       3.1
     161.0       4.7
     162.0       1.0
     163.0       4.9
     164.0       1.9
     165.0       1.7
     168.0       2.0
     175.0       2.0
     176.0       2.1
     177.0       1.3
     179.0      64.9
     180.0       8.5
     181.0      23.4
     182.0       3.1
     183.0       2.2
     185.0       3.7
     189.0       1.0
     191.0       1.4
     195.0       2.5
     199.0       2.2
     201.0       1.0
     203.0       1.4
     209.0      25.7
     210.0      14.0
     211.0       2.5
     219.0       8.7
     220.0       1.0
     221.0       3.2
     224.0       2.2
     225.0       9.0
     226.0       1.4
     227.0       3.1
     242.0       1.2
     243.0       1.2
     245.0      92.0
     246.0      11.9
     247.0      32.8
     248.0       4.1
     249.0       1.3
     260.0     100.0
     261.0      14.0
     262.0      36.3
     263.0       4.8
     264.0       1.4
     273.0       1.2
     303.0       1.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₆ Cl F₅ Si	0.05 ml : 0.5 ml CDCl₃
chlorodimethyl(pentafluorophenyl)silane

    Assign.     Shift(ppm)

      A             0.835
     
     J(F-19,A)=1.9HZ

     Hz     ppm     Int.

     80.31   0.897     56
     78.44   0.876    114
     76.69   0.857    605
     74.81   0.836   1000
     72.94   0.815    533
     71.06   0.794     62
     69.19   0.773     34

liquid film