20103-09-7

2,5-二-氯-1,4-苯二胺(20103-09-7)质谱(MS)

产品名称:2,5-二-氯-1,4-苯二胺

CAS:20103-09-7

分子式:C6H6Cl2N2

分子量: 177.03

InChI:InChI=1S/C6H6Cl2N2/c7-3-1-5(9)4(8)2-6(3)10/h1-2H,9-10H2

InChIKey: QAYVHDDEMLNVMO-UHFFFAOYSA-N

Smiles:C1(N)=CC(Cl)=C(N)C=C1Cl

Mass

MS-IW-9138          
2,5-dichloro-p-phenylenediamine
C6H6Cl2N2           (Mass of molecular ion:    176)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      28.0       5.0
      36.0       1.1
      38.0       1.1
      40.0       1.3
      50.0       1.6
      51.0       5.1
      52.0      12.7
      52.5       1.2
      53.0       6.0
      54.0       1.5
      56.5       1.0
      61.0       1.4
      62.0       1.9
      63.0       1.0
      70.0       5.2
      70.5       1.3
      71.0       1.8
      75.0       1.2
      76.0       4.2
      77.0       1.8
      78.0      14.7
      79.0       2.4
      85.0       1.1
      86.0       1.4
      87.0       2.2
      88.0      12.1
      89.0       7.6
      90.0       1.6
     105.0       6.4
     106.0       2.7
     112.0       2.5
     113.0       9.5
     114.0      12.5
     115.0       3.8
     116.0       4.3
     124.0       1.3
     139.0       4.2
     140.0       8.0
     141.0      13.1
     142.0       3.5
     143.0       3.9
     148.0       6.2
     150.0       4.1
     175.0      10.3
     176.0     100.0
     177.0      14.2
     178.0      64.0
     179.0       5.7
     180.0      10.4

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₆ Cl₂ N₂	0.038 g : 0.5 ml DMSO-d₆
2,5-dichloro-p-phenylenediamine

    Assign.     Shift(ppm)

      A             6.759
      B             4.68

     Hz     ppm     Int.

   2701.54   6.760   1000
   1868.53   4.676    603

in DMSO-d6

KBr disc

nujol mull

更多供应商

陕西缔都医药化工有限公司黄金产品

湖北中隆康盛精细化工有限公司黄金产品