2312-23-4

3-氯苯肼盐酸盐(2312-23-4)红外图谱(IR1)

产品名称:3-氯苯肼盐酸盐

CAS:2312-23-4

分子式:C6H8Cl2N2

分子量: 179.05

Mass

MS-IW-9063          
m-chlorophenylhydrazine hydrochloride
C6H7ClN2 HCl        (Mass of molecular ion:    142)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      16.0       1.2
      17.0       3.1
      18.0      10.4
      27.0       1.3
      28.0       6.3
      29.0       4.8
      30.0       1.2
      31.0       3.5
      35.0       4.8
      36.0      47.6
      37.0       3.8
      38.0      19.0
      39.0       6.1
      40.0       1.1
      41.0       1.4
      44.5       1.3
      45.5       2.2
      49.0       1.6
      50.0       8.7
      51.0      10.3
      52.0       3.8
      53.0       4.3
      61.0       2.6
      62.0       4.2
      63.0      12.7
      63.5       1.3
      64.0       6.2
      65.0       6.2
      71.0       3.8
      72.0       1.8
      73.0       5.8
      74.0       4.7
      75.0      14.2
      76.0       3.6
      77.0      31.3
      78.0       4.6
      79.0       1.7
      80.0       4.4
      85.0       1.8
      87.0       1.1
      89.0       2.4
      90.0      14.8
      91.0       9.9
      92.0       4.9
      98.0       1.4
      99.0      29.3
     100.0       4.1
     101.0       9.5
     102.0       1.2
     107.0      27.8
     108.0       2.3
     111.0      11.7
     112.0      18.6
     113.0       6.6
     114.0       7.1
     115.0       1.3
     125.0      13.6
     126.0      26.0
     127.0      30.2
     128.0      10.3
     129.0       8.6
     140.0       3.6
     141.0       4.8
     142.0     100.0
     143.0       8.5
     144.0      31.7
     145.0       2.4

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₇ Cl N₂	0.040 g : 0.5 ml DMSO-d₆
m-chlorophenylhydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.5
      B             8.7
      C             7.289
      D             7.119
      E     *1      6.98
      F     *1      6.96

     Hz     ppm     Int.

   4211.43  10.538    511
   3471.68   8.687     39
   2921.75   7.311    497
   2918.55   7.303     26
   2913.67   7.291   1000
   2905.58   7.271    649
   2847.29   7.125    554
   2845.15   7.120    997
   2843.17   7.115    598
   2795.72   6.996    475
   2794.34   6.992    373
   2793.43   6.990    404
   2787.93   6.976    792
   2787.32   6.975    811
   2785.95   6.971    817
   2785.19   6.970    739
   2780.00   6.957    437
   2779.24   6.955    430
   2778.02   6.952    452
   2777.25   6.950    374

in DMSO-d6