2406-34-0

1,1-二氯硅杂环己烷(2406-34-0)红外图谱(IR1)

产品名称:1,1-二氯硅杂环己烷

CAS:2406-34-0

分子式:C5H10Cl2Si

分子量: 169.12

InChI:InChI=1S/C5H10Cl2Si/c6-8(7)4-2-1-3-5-8/h1-5H2

InChIKey: KPYXTYWOSWVJBL-UHFFFAOYSA-N

Smiles:[Si]1(Cl)(Cl)CCCCC1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-6044          
1,1-dichloro-1-silacyclohexane
C5H10Cl2Si          (Mass of molecular ion:    168)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.1
      18.0       2.3
      26.0       1.8
      27.0      11.2
      28.0       1.5
      29.0       5.1
      36.0       2.4
      38.0       1.7
      39.0      20.4
      40.0       3.7
      41.0      31.4
      42.0      18.4
      43.0      10.7
      44.0       1.4
      47.0       1.0
      51.0       1.2
      53.0       2.6
      54.0      10.5
      55.0      11.9
      56.0       2.3
      57.0       3.3
      63.0      29.8
      64.0       2.8
      65.0      11.8
      66.0       1.5
      67.0       3.4
      68.0       2.5
      69.0      15.4
      70.0       8.5
      71.0       1.8
      77.0       2.3
      78.0       1.6
      79.0       2.0
      80.0       1.6
      81.0       1.0
      90.0       1.0
      91.0       1.7
      93.0       1.6
      95.0       2.0
      96.0       2.7
      97.0       2.0
      98.0      11.2
      99.0      19.1
     100.0       8.4
     101.0      12.8
     102.0       2.2
     103.0       3.7
     104.0       7.5
     105.0       3.7
     106.0       3.2
     107.0       1.7
     108.0       2.0
     109.0       1.1
     111.0       1.6
     112.0      56.9
     113.0      14.1
     114.0      38.2
     115.0       9.0
     116.0       7.8
     117.0       5.9
     119.0       2.0
     123.0       1.1
     124.0       2.0
     125.0      27.5
     126.0      13.7
     127.0      56.2
     128.0      12.2
     129.0      30.4
     130.0       4.1
     131.0       6.6
     132.0      29.0
     133.0       6.0
     134.0      10.5
     135.0       2.4
     136.0       2.3
     137.0       1.1
     138.0       1.2
     139.0      12.9
     140.0     100.0
     141.0      16.7
     142.0      66.2
     143.0       7.7
     144.0      12.3
     145.0       1.5
     152.0       1.3
     153.0       2.8
     155.0       1.8
     161.0       1.4
     163.0       1.2
     167.0       1.2
     168.0      42.7
     169.0       5.4
     170.0      28.2
     171.0       3.6
     172.0       5.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₅ H₁₀ Cl₂ Si	0.05 ml : 0.5 ml CDCl₃
1,1-dichloro-1-silacyclohexane

    Assign.     Shift(ppm)

      A             1.839
      B             1.497
      C             1.197

     Hz     ppm     Int.

    747.56   1.871    271
    741.82   1.857    389
    740.97   1.855    405
    739.01   1.850    347
    738.28   1.848    374
    735.96   1.842    549
    734.50   1.838    511
    731.69   1.831    373
    731.08   1.830    367
    729.61   1.826    403
    728.64   1.824    409
    722.66   1.809    278
    609.50   1.526    187
    606.81   1.519    145
    605.47   1.516    110
    603.76   1.511    285
    601.07   1.504    203
    598.14   1.497    481
    595.46   1.490    194
    594.24   1.487    154
    592.77   1.484    205
    592.04   1.482    188
    589.72   1.476    123
    586.79   1.469    143
    485.23   1.215   1000
    480.83   1.204    372
    478.39   1.198    983
    471.68   1.181    862

in CDCl3