2,3-二氯硝基苯(3209-22-1)核磁图(¹³CNMR)

Mass

MS-NW-8884          
1,2-dichloro-3-nitrobenzene
C6H3Cl2NO2          (Mass of molecular ion:    191)

   Source Temperature: 280 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      28.0       3.5
      30.0      40.2
      36.0       3.2
      37.0       3.9
      38.0       3.2
      39.0       1.9
      46.0       1.0
      49.0       4.3
      50.0       8.5
      51.0       2.8
      61.0       4.4
      62.0       3.1
      63.0       6.7
      72.0       2.8
      73.0      12.5
      74.0      42.4
      75.0      39.2
      76.0       2.7
      83.0       2.3
      84.0      17.7
      85.0      11.4
      86.0       6.5
      87.0       4.2
      88.0       1.0
      97.0       2.4
      98.0       1.9
     107.0       3.2
     108.0       2.8
     109.0      94.5
     110.0      18.5
     111.0      31.0
     112.0       5.8
     119.0       2.4
     121.0       1.7
     126.0       2.5
     128.0       1.1
     133.0      67.6
     134.0       3.9
     135.0      43.7
     136.0       2.5
     137.0       7.1
     144.0       1.4
     145.0     100.0
     146.0       7.5
     147.0      63.6
     148.0       4.4
     149.0      10.3
     161.0      22.8
     162.0       1.6
     163.0      14.7
     164.0       1.0
     165.0       2.5
     175.0       2.1
     177.0       1.4
     191.0      96.7
     192.0       6.9
     193.0      62.4
     194.0       4.4
     195.0      10.3

Assign. Shift(ppm) A 7.70 B 7.69 C 7.37 A AND B WERE CONFIRMED BY LAOCN PROGRAM.

     Hz     ppm     Int.

    695.38   7.765    254
    694.63   7.757    447
    693.63   7.745    402
    692.81   7.736    334
    686.50   7.666    926
    685.75   7.657   1000
    667.63   7.455    575
    660.56   7.376    315
    658.69   7.355    227
    651.63   7.276    274