3237-62-5

1-乙基-2-甲基-5,6-二氯苯并咪唑(3237-62-5)质谱(MS)

产品名称:1-乙基-2-甲基-5,6-二氯苯并咪唑

CAS:3237-62-5

分子式:C10H10Cl2N2

分子量: 229.11

InChI:InChI=1S/C10H10Cl2N2/c1-3-14-6(2)13-9-4-7(11)8(12)5-10(9)14/h4-5H,3H2,1-2H3

InChIKey: IVVLMQPTQOLYDX-UHFFFAOYSA-N

Smiles:C1(C)N(CC)C2=CC(Cl)=C(Cl)C=C2N=1

Mass

MS-IW-9742          
5,6-dichloro-1-ethyl-2-methylbenzimidazole
C10H10Cl2N2         (Mass of molecular ion:    228)

   Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      27.0       4.5
      28.0       3.0
      29.0       4.5
      41.0       1.8
      42.0       3.0
      50.0       1.1
      51.0       1.1
      52.0       1.4
      61.0       1.8
      62.0       2.5
      63.0       1.2
      72.0       1.3
      73.0       2.1
      74.0       3.1
      75.0       3.5
      76.0       2.0
      84.0       1.1
      85.0       1.0
      86.0       1.2
      87.0       1.6
      88.0       5.5
      89.0       2.8
      92.5       2.6
      93.5       1.8
      96.0       1.1
      97.0       5.9
      98.0       1.8
      99.0       2.8
     100.0       2.7
     101.0       1.0
     102.0       1.6
     106.0       8.6
     106.5       3.2
     107.0       6.8
     107.5       1.9
     108.0       1.8
     109.0       6.0
     110.0       1.9
     111.0       2.5
     112.0       1.0
     113.0       1.3
     114.0      10.0
     114.5       1.2
     115.0       6.1
     116.0       2.2
     117.0       1.0
     123.0       1.7
     124.0       3.2
     125.0       1.6
     126.0       1.2
     133.0       1.7
     134.0       1.0
     135.0       1.3
     136.0       1.8
     137.0       2.2
     138.0       1.4
     143.0       1.2
     144.0       1.2
     145.0       3.8
     146.0       1.4
     147.0       2.5
     150.0       1.3
     151.0       3.4
     152.0       1.7
     153.0       1.4
     158.0       3.4
     159.0       1.4
     160.0       5.7
     161.0       1.2
     162.0       2.8
     164.0       1.2
     165.0       2.9
     172.0       1.8
     174.0       1.1
     177.0       2.4
     178.0      11.9
     179.0       2.2
     180.0       3.9
     186.0       1.8
     187.0       1.7
     188.0       1.2
     189.0       1.0
     193.0       2.0
     199.0       7.1
     200.0       4.3
     201.0       5.0
     202.0       2.8
     203.0       1.1
     213.0      93.4
     214.0      10.3
     215.0      60.1
     216.0       6.5
     217.0      10.1
     218.0       1.0
     227.0       4.0
     228.0     100.0
     229.0      14.3
     230.0      64.1
     231.0       8.1
     232.0      10.6
     233.0       1.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₀ Cl₂ N₂	0.040 g : 0.5 ml CDCl₃
5,6-dichloro-1-ethyl-2-methylbenzimidazole

    Assign.     Shift(ppm)

      A             7.722
      B             7.346
      C             4.085
      D             2.578
      E             1.383

     Hz     ppm     Int.

   3086.18   7.723    336
   2936.04   7.347    330
   1643.68   4.113     71
   1636.35   4.095    222
   1629.03   4.077    223
   1621.70   4.058     71
   1033.45   2.586     39
   1030.27   2.578   1000
    560.06   1.402    237
    552.86   1.384    486
    545.53   1.366    230

in CDCl3