3518-83-0

N-乙基-4-羟基哌啶(3518-83-0)红外图谱(IR1)

产品名称:N-乙基-4-羟基哌啶

CAS:3518-83-0

分子式:C7H15NO

分子量: 129.2

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-7560          
1-ethyl-4-piperidinol
C7H15NO             (Mass of molecular ion:    129)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       2.9
      18.0       1.5
      26.0       1.1
      27.0       8.9
      28.0      11.9
      29.0       9.5
      30.0       7.2
      31.0       2.1
      39.0       2.3
      41.0       5.6
      42.0      30.7
      43.0       5.3
      44.0      49.6
      45.0       2.2
      53.0       3.1
      54.0       2.9
      55.0       9.7
      56.0      13.8
      57.0      21.0
      58.0      11.5
      68.0       1.4
      69.0       1.3
      70.0       5.2
      71.0       4.5
      72.0       2.7
      82.0       1.4
      84.0      17.9
      85.0       2.1
      96.0       3.5
     100.0       1.1
     110.0       5.4
     112.0       7.8
     114.0     100.0
     115.0       7.6
     128.0      12.6
     129.0      23.4
     130.0       2.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₅ N O	0.05 ml : 0.5 ml CDCl₃
1-ethyl-4-piperidinol

    Assign.     Shift(ppm)

      A             4.08
      B             3.609
      C             2.794
      D             2.392
      E             2.089
      F             1.878
      G             1.599
      J             1.077

     Hz     ppm     Int.

   1467.90   3.673     30
   1467.41   3.672     30
   1463.99   3.664     46
   1459.35   3.652     61
   1454.96   3.641     73
   1450.68   3.630     57
   1447.51   3.622     37
   1445.92   3.618     41
   1122.07   2.808    109
   1116.09   2.793    103
   1115.60   2.792    103
   1110.84   2.780    112
   1110.60   2.779    112
    970.09   2.428     37
    967.16   2.421    161
    962.89   2.410     55
    959.84   2.402    480
    952.64   2.384    494
    945.43   2.366    169
    844.97   2.115     78
    844.73   2.114     78
    834.72   2.089    123
    824.71   2.064     72
    824.46   2.063     72
    761.23   1.905     62
    757.81   1.897    110
    753.91   1.887    113
    750.24   1.878     98
    748.54   1.873    104
    744.87   1.864    133
    740.97   1.855    127
    656.13   1.642     75
    652.47   1.633     79
    646.12   1.617    110
    643.07   1.610    154
    639.65   1.601     84
    636.72   1.594     83
    633.18   1.585    138
    630.25   1.578     91
    623.78   1.561     55
    620.12   1.552     50
    440.80   1.103     76
    437.74   1.096    527
    430.54   1.078   1000
    423.22   1.059    511
    420.41   1.052     68

in CDCl3