4-氟氯苄(352-11-4)Raman光谱
InChI:InChI=1S/C7H6ClF/c8-5-6-1-3-7(9)4-2-6/h1-4H,5H2
InChIKey: IZXWCDITFDNEBY-UHFFFAOYSA-N
Smiles:C1(CCl)=CC=C(F)C=C1
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Mass
MS-NW-7765
p-fluorobenzyl chloride
C7H6ClF (Mass of molecular ion: 144)
Source Temperature: 240 °C
Sample Temperature: 140 °C
Reservoir, 75 eV
31.0 1.4
38.0 1.1
39.0 2.7
44.0 1.3
50.0 2.5
51.0 1.9
57.0 5.4
59.0 1.1
61.0 1.3
62.0 2.3
63.0 3.8
81.0 3.0
82.0 1.0
83.0 11.9
89.0 1.7
107.0 6.5
108.0 2.5
109.0 100.0
110.0 7.9
143.0 3.0
144.0 20.7
145.0 2.5
146.0 6.7
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C7 H6 Cl F
|
0.05 ml : 0.5 ml CDCl3
|
| p-fluorobenzyl chloride
|
 |
Assign. Shift(ppm)
A 7.323
B 7.010
C 4.525
|
Hz ppm Int.
2936.89 7.349 40
2933.84 7.342 286
2931.64 7.336 125
2928.59 7.328 306
2927.25 7.325 179
2926.76 7.324 173
2925.05 7.320 317
2922.00 7.312 143
2919.80 7.306 305
2916.75 7.299 46
2812.87 7.039 52
2809.94 7.032 366
2807.74 7.026 117
2803.22 7.015 150
2801.27 7.010 601
2799.19 7.005 138
2794.68 6.993 117
2792.60 6.988 314
2789.55 6.980 43
1808.35 4.525 1000
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| 1H NMR |
89.56 MHz |
| C7 H6 Cl F
|
0.05 ml : 0.5 ml CDCl3
|
| p-fluorobenzyl chloride
|
|
Assign. Shift(ppm)
A 7.304
B 7.011
C 4.517
|
Hz ppm Int.
662.94 7.403 154
660.75 7.378 84
657.56 7.343 190
654.06 7.304 306
651.13 7.271 131
648.75 7.244 291
646.06 7.214 61
644.75 7.200 58
637.81 7.122 64
635.13 7.092 333
632.81 7.066 103
628.50 7.018 112
626.56 6.996 465
624.38 6.972 115
621.44 6.939 37
619.94 6.923 82
617.81 6.899 178
404.63 4.518 1000