36171-39-8

1-叠氮基芘(36171-39-8)核磁图(¹³CNMR)

产品名称:1-叠氮基芘

CAS:36171-39-8

分子式:

分子量:

InChI:InChI=1S/C16H9N3/c17-19-18-14-9-7-12-5-4-10-2-1-3-11-6-8-13(14)16(12)15(10)11/h1-9H

InChIKey: BMNGOGRNWBJJKB-UHFFFAOYSA-N

Smiles:C1(N=[N+]=[N-])=C2C3=C4C(C=C2)=CC=CC4=CC=C3C=C1

¹HNMR

¹³CNMR

ESR

Mass

MS2004-02557WA      
1-pyrenyl azide
C16H9N3             (Mass of molecular ion:    243)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 70 eV

      28.0      11.2
      62.0       1.3
      63.0       2.4
      68.0       1.2
      72.0       1.5
      74.0       2.0
      75.0       1.2
      80.0       1.2
      80.5       1.9
      81.0       3.9
      81.5       2.1
      86.0       2.0
      87.0       3.2
      88.0       1.0
      93.0       7.5
      93.5      37.6
      94.0      30.3
      94.5       8.0
      95.0       1.3
      98.0       1.5
      99.0       1.7
     100.0       3.3
     100.5       1.1
     106.5       2.5
     107.0       5.5
     107.5      34.0
     108.0       6.1
     108.5       3.5
     110.0       1.1
     111.0       1.4
     161.0       1.9
     162.0       1.7
     163.0       3.3
     164.0       1.7
     185.0       1.4
     186.0       3.0
     187.0      12.9
     188.0      11.1
     189.0      10.7
     190.0       2.0
     200.0       1.4
     201.0       1.0
     212.0       6.5
     213.0       5.9
     214.0      82.0
     215.0     100.0
     216.0      19.3
     217.0      17.3
     218.0       2.9
     243.0      22.8
     244.0       4.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₆H₉N₃	22 mg : 0.5 ml CDCl₃
1-pyrenyl azide

    Assign.     Shift(ppm)

     A           8.193
     B *1        8.113
     C *1        8.106
     D           8.052
     E           7.99
     F           7.962
     G *2        7.94
     J *2        7.92
     K           7.698

     Hz     ppm     Int.

   3280.16   8.205    516
   3271.00   8.182    646
   3247.44   8.124    356
   3245.12   8.118    332
   3237.43   8.098    470
   3223.27   8.063    516
   3215.09   8.043    571
   3200.57   8.006    595
   3191.17   7.983    857
   3183.35   7.963    659
   3175.79   7.944    355
   3170.42   7.931   1000
   3161.50   7.909    170
   3081.18   7.708    731
   3073.00   7.687    648

in CDCl3

Spectral Code: ESR : PHOTOLYSIS, IN BENZENE, 77K

更多供应商

Hangzhou Sage Chemical Co., Ltd.

深圳市丽晶生化科技有限公司

河南阿尔法化工有限公司

Jilin Chinese Academy of Sciences-yanshen Technology

上海博拓生物科技有限公司

吉林中科研伸科技有限公司

1-叠氮基芘(36171-39-8)核磁图(13CNMR)

1-叠氮基芘(36171-39-8)核磁图(¹³CNMR)