37529-30-9

4-癸基苯胺(37529-30-9)核磁图(¹³CNMR)

产品名称:4-癸基苯胺

CAS:37529-30-9

分子式:C16H27N

分子量: 233.39

Mass

MS-NW-7460          
p-decylaniline
C16H27N             (Mass of molecular ion:    233)

   Source Temperature: 240 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      27.0       1.1
      28.0       1.1
      29.0       2.0
      39.0       1.0
      41.0       2.5
      43.0       1.8
      55.0       1.0
      77.0       2.2
      78.0       1.1
      79.0       1.3
      93.0       1.0
     106.0     100.0
     107.0       8.7
     119.0       1.6
     120.0       1.1
     233.0      13.8
     234.0       2.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₆ H₂₇ N	0.036 g : 0.5 ml CDCl₃
p-decylaniline

    Assign.     Shift(ppm)

      A             6.97
      B             6.62
      C             3.5
      D             2.48
      E             1.57
      F          1.34 to 1.15
      G             0.88

     Hz     ppm     Int.

    628.25   7.015     94
    626.13   6.992     48
    624.63   6.975     43
    619.88   6.922    146
    617.31   6.893     37
    596.38   6.660    138
    594.25   6.636     55
    589.75   6.585     51
    588.00   6.566     81
    230.13   2.570     40
    228.38   2.551     33
    227.94   2.546     33
    223.25   2.493     79
    215.63   2.408     66
    145.94   1.630     34
    142.63   1.593     41
    142.38   1.590     41
    140.31   1.567     49
    139.63   1.560     49
    137.25   1.533     51
    136.69   1.527     50
    135.13   1.509     46
    134.00   1.497     46
    133.31   1.489     46
    131.13   1.465     51
    130.06   1.453     53
    129.75   1.449     53
    125.81   1.405     71
    112.44   1.256   1000
     93.56   1.045     33
     92.44   1.033     33
     90.44   1.010     31
     83.44   0.932     92
     82.31   0.920     83
     80.94   0.904     88
     78.56   0.878    186
     75.75   0.846     69
     72.81   0.813     61

in CDCl3