38775-38-1

十六烷基磺酰氯(38775-38-1)质谱(MS)

产品名称:十六烷基磺酰氯

CAS:38775-38-1

分子式:C16H33ClO2S

分子量: 324.95

Mass

MS-NW-9995          
1-hexadecanesulfonyl chloride
C16H33ClO2S         (Mass of molecular ion:    324)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       1.8
      27.0       4.8
      28.0       2.2
      29.0      16.1
      36.0       2.3
      39.0       4.3
      40.0       1.0
      41.0      42.2
      42.0      11.2
      43.0      76.7
      44.0       2.7
      48.0       1.3
      53.0       2.4
      54.0       5.1
      55.0      56.0
      56.0      27.8
      57.0     100.0
      58.0       4.8
      64.0       4.1
      67.0       7.6
      68.0      14.1
      69.0      60.9
      70.0      29.5
      71.0      61.2
      72.0       3.5
      81.0       6.2
      82.0      21.5
      83.0      68.2
      84.0      22.2
      85.0      36.1
      86.0       2.4
      91.0       2.0
      95.0       3.9
      96.0      11.3
      97.0      63.8
      98.0      16.7
      99.0       9.9
     105.0       1.0
     109.0       2.0
     110.0       5.9
     111.0      40.2
     112.0      13.0
     113.0       5.5
     123.0       1.3
     124.0       3.8
     125.0      20.8
     126.0       8.9
     127.0       3.6
     138.0       2.7
     139.0      10.1
     140.0       6.4
     141.0       2.7
     152.0       1.9
     153.0       6.2
     154.0       5.0
     155.0       1.9
     166.0       1.2
     167.0       4.4
     168.0       3.7
     169.0       1.2
     181.0       3.2
     182.0       2.3
     195.0       2.5
     196.0       5.4
     197.0       1.0
     224.0       8.4
     225.0       1.9
     253.0       1.7
     271.0       4.9
     289.0       1.3
     307.0       1.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₆ H₃₃ Cl O₂ S	0.031 g : 0.5 ml CDCl₃
1-hexadecanesulfonyl chloride

    Assign.     Shift(ppm)

      A             3.658
      B             2.040
      C             1.484
      D             1.35
      E             1.26
      F             0.880

     Hz     ppm     Int.

   1469.97   3.679     64
   1462.16   3.659     57
   1454.22   3.639     67
    823.61   2.061     30
    815.67   2.041     51
    808.11   2.023     34
    594.97   1.489     40
    587.40   1.470     33
    538.94   1.349     35
    537.35   1.345     34
    533.69   1.336     42
    527.10   1.319     60
    519.53   1.300     78
    503.54   1.260   1000
    358.64   0.898     62
    352.05   0.881    158
    345.09   0.864     69

in CDCl3