41830-80-2

5,9-二氨基苯并[A]吩恶嗪-7-高氯酸盐(41830-80-2)红外图谱(IR1)

产品名称:5,9-二氨基苯并[A]吩恶嗪-7-高氯酸盐

CAS:41830-80-2

分子式:C16H12ClN3O5

分子量: 361.74

Mass

MS-NW-7464          
cresyl violet perchlorate
C16H12ClN3O5        (Mass of molecular ion:    361)

   Source Temperature: 230 °C
   Sample Temperature: 250 °C
   Direct, 75 eV

      17.0       2.9
      18.0      12.9
      28.0       4.8
      35.0       1.2
      36.0       8.6
      38.0       2.9
      39.0       2.5
      41.0       2.4
      44.0      12.8
      50.0       1.0
      51.0       1.9
      52.0       2.6
      62.0       1.4
      63.0       3.3
      64.0       2.3
      65.0       1.4
      66.0       2.0
      67.0       1.9
      75.0       1.5
      76.0       2.4
      77.0       1.2
      78.0       1.6
      79.0       2.7
      80.0       1.0
      87.0       1.0
      88.0       1.2
      89.0       2.1
      89.5       1.1
      90.0       1.1
      91.0       2.8
     102.0       1.6
     102.5       1.1
     103.0       2.7
     104.0       1.0
     113.0       1.7
     114.0       1.0
     117.0      12.5
     117.5       2.3
     121.0       2.3
     128.0       1.1
     130.0       1.1
     130.5       3.5
     139.0       1.0
     140.0       1.5
     151.0       1.1
     177.0       1.0
     178.0       1.4
     179.0       1.3
     205.0       5.8
     206.0       2.0
     232.0       1.6
     233.0       2.1
     234.0      20.3
     235.0       4.4
     260.0       9.2
     261.0     100.0
     262.0      19.2
     263.0       2.2
     287.0       2.6

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₆ H₁₂ Cl N₃ O₅	0.046 g : 0.5 ml DMSO-d₆
cresyl violet perchlorate

    Assign.     Shift(ppm)

      A     *1      9.70
      B     *1      9.61
      C     *2      8.503
      D     *2      8.269
      E             7.87
      F     *3      7.836
      G     *3      7.738
      J             7.601
      K             6.956
      L             6.581
      M             6.580

     Hz     ppm     Int.

   3876.80   9.701     60
   3839.57   9.608     57
   3403.02   8.516    197
   3401.95   8.513    199
   3394.93   8.495    221
   3393.86   8.493    208
   3309.02   8.280    177
   3300.78   8.260    193
   3100.43   7.758    128
   3099.21   7.755    129
   3092.19   7.738    190
   3091.13   7.735    146
   3085.17   7.720     95
   3083.95   7.717     91
   3042.76   7.614    439
   3033.75   7.592    494
   2785.95   6.971    207
   2783.66   6.966    205
   2776.95   6.949    198
   2774.66   6.943    210
   2631.38   6.585    540
   2629.85   6.581   1000

KBr disc