4606-07-9

环丙基甲酸乙酯(4606-07-9)核磁图(¹HNMR)

产品名称:环丙基甲酸乙酯

CAS:4606-07-9

分子式:C6H10O2

分子量: 114.14

InChI:InChI=1S/C6H10O2/c1-2-8-6(7)5-3-4-5/h5H,2-4H2,1H3

InChIKey: LDDOSDVZPSGLFZ-UHFFFAOYSA-N

Smiles:C1(C(OCC)=O)CC1

Mass

MS-NW-6445          
ethyl cyclopropanecarboxylate
C6H10O2             (Mass of molecular ion:    114)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.0
      26.0       2.0
      27.0       9.3
      28.0       1.1
      29.0      24.0
      31.0       1.3
      38.0       1.7
      39.0      17.1
      40.0       3.5
      41.0      33.9
      42.0       7.4
      43.0       2.9
      45.0       6.2
      55.0       3.7
      57.0       1.0
      58.0       5.7
      59.0       1.0
      68.0       5.0
      69.0     100.0
      70.0       5.2
      71.0       2.7
      73.0       2.8
      83.0       1.2
      85.0       6.6
      86.0      23.2
      87.0      12.3
      99.0       1.6
     114.0       3.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₁₀ O₂	0.05 ml : 0.5 ml CDCl₃
ethyl cyclopropanecarboxylate

    Assign.     Shift(ppm)

      A             4.130
      B             1.596
      C             1.263
      D             0.958
      E             0.845

     Hz     ppm     Int.

   1661.25   4.157    232
   1654.17   4.140    592
   1646.97   4.122    618
   1639.89   4.104    244
    650.39   1.628     58
    645.75   1.616    117
    642.46   1.608    121
    641.11   1.605     81
    637.70   1.596    230
    634.28   1.588     83
    633.18   1.585    132
    629.64   1.576    131
    625.00   1.564     70
    511.96   1.282    634
    509.40   1.275     38
    504.76   1.264   1000
    497.68   1.246    643
    399.05   0.999     91
    394.29   0.987    292
    391.48   0.980    351
    390.38   0.977    230
    389.65   0.975    270
    387.94   0.971    192
    386.84   0.968    334
    383.42   0.960    123
    382.81   0.958    106
    346.19   0.867    120
    345.58   0.865    110
    342.41   0.857    341
    339.48   0.850    243
    338.38   0.847    214
    334.35   0.837    341
    331.30   0.829    244
    327.03   0.819     93

in CDCl3