4963-47-7

三(3-氨基丙基)胺(4963-47-7)红外图谱(IR1)

产品名称:三(3-氨基丙基)胺

CAS:4963-47-7

分子式:C9H24N4

分子量: 188.31

InChI:InChI=1S/C9H24N4/c10-4-1-7-13(8-2-5-11)9-3-6-12/h1-12H2

InChIKey: QMXSDTGNCZVWTB-UHFFFAOYSA-N

Smiles:C(N(CCCN)CCCN)CCN

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-7200          
N,N-bis(3-aminopropyl)trimethylenediamine
C9H24N4             (Mass of molecular ion:    188)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.0
      16.0       2.8
      17.0       5.8
      18.0      17.5
      26.0       2.1
      27.0       5.2
      28.0      19.5
      29.0       3.3
      30.0      29.4
      31.0       1.9
      32.0       1.8
      39.0       2.6
      40.0       1.9
      41.0      10.8
      42.0      12.7
      43.0       8.3
      44.0      33.2
      45.0       1.9
      47.0       1.9
      52.0       1.2
      54.0       2.9
      55.0       2.7
      56.0      12.9
      57.0       9.6
      58.0     100.0
      59.0       6.2
      68.0       2.7
      69.0       1.6
      70.0      17.5
      71.0       5.5
      72.0      16.8
      73.0       3.0
      75.0       1.9
      77.0       1.1
      79.0       3.7
      80.0       1.1
      81.0      14.0
      82.0       2.2
      83.0       1.6
      84.0      13.3
      85.0       6.8
      86.0       1.6
      87.0       4.4
      96.0       2.7
      97.0       1.0
      98.0       5.7
      99.0       4.3
     101.0      12.1
     102.0       1.0
     113.0       9.2
     114.0       1.6
     115.0       5.1
     127.0      17.9
     128.0       1.9
     130.0       3.8
     131.0       4.0
     132.0       3.3
     141.0       1.5
     142.0       1.3
     144.0      25.7
     145.0       3.4
     155.0       2.3
     158.0       1.3
     188.0       7.6
     189.0       1.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₂₄ N₄	0.05 ml : 0.5 ml CDCl₃
N,N-bis(3-aminopropyl)trimethylenediamine

    Assign.     Shift(ppm)

      A             2.713
      B             2.450
      C             1.584
      D             1.42

     Hz     ppm     Int.

   1091.31   2.731    634
   1084.47   2.714   1000
   1077.51   2.697    637
   1071.90   2.683     22
    986.33   2.468    536
    979.25   2.451    593
    971.92   2.432    553
    650.02   1.627     33
    646.97   1.619    181
    640.01   1.602    433
    632.81   1.584    518
    625.73   1.566    393
    618.77   1.549    149
    565.55   1.416    259

in CDCl3