N-(萘-2-基)乙酰胺(581-97-5)红外图谱(IR1)
InChI:InChI=1S/C12H11NO/c1-9(14)13-12-7-6-10-4-2-3-5-11(10)8-12/h2-8H,1H3,(H,13,14)
InChIKey: DIEOESIZLAHURK-UHFFFAOYSA-N
Smiles:C(NC1=CC=C2C(=C1)C=CC=C2)(=O)C
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Mass
MS-NW-1442
N-(2-naphthyl)acetamide
C12H11NO (Mass of molecular ion: 185)
Source Temperature: 250 °C
Sample Temperature: 170 °C
Reservoir, 75 eV
14.0 1.0
15.0 1.7
17.0 2.6
18.0 11.9
39.0 2.3
43.0 13.5
44.0 3.2
50.0 1.4
51.0 1.8
62.0 1.6
63.0 3.6
65.0 1.8
74.0 1.1
75.0 1.6
76.0 1.0
77.0 1.2
88.0 1.3
89.0 3.4
113.0 1.6
114.0 2.9
115.0 24.7
116.0 7.5
117.0 1.1
126.0 1.3
127.0 2.0
140.0 2.0
141.0 1.4
142.0 2.8
143.0 100.0
144.0 12.3
145.0 1.0
185.0 41.6
186.0 6.0
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C12 H11 N O
|
0.020 g : 0.5 ml CDCl3
|
| N-(2-naphthyl)acetamide
|
 |
Assign. Shift(ppm)
A 8.173
B 7.90
C 7.75
D 7.74
E 7.73
F 7.46
G *1 7.42
J *1 7.39
K 2.197
J(A,F)=1.8HZ.
|
Hz ppm Int.
3267.21 8.176 133
3265.38 8.171 132
3154.17 7.893 51
3101.20 7.760 100
3095.70 7.747 150
3092.16 7.738 155
3087.16 7.725 149
3082.89 7.714 101
2984.62 7.469 99
2982.42 7.463 98
2975.71 7.446 96
2973.63 7.441 112
2967.41 7.426 93
2966.06 7.422 92
2959.72 7.406 96
2957.89 7.402 144
2956.18 7.397 99
2949.71 7.381 85
2948.49 7.378 81
2942.99 7.364 38
2941.65 7.361 33
878.17 2.198 1000
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| 1H NMR |
89.56 MHz |
| C12 H11 N O
|
0.045 g : 0.5 ml CDCl3
|
| N-(2-naphthyl)acetamide
|
|
Assign. Shift(ppm)
A 8.15
B 8.04
C 7.83 to 7.58
D 7.54 to 7.20
E 2.171
|
Hz ppm Int.
730.75 8.160 69
730.19 8.154 70
729.25 8.143 74
729.13 8.142 74
697.69 7.791 44
695.31 7.764 88
692.94 7.738 55
691.69 7.724 62
689.50 7.699 65
687.06 7.672 170
671.94 7.503 74
669.88 7.480 91
668.00 7.459 32
665.88 7.436 118
665.06 7.426 112
663.31 7.407 103
661.13 7.382 105
660.19 7.372 79
658.19 7.350 62
655.88 7.324 92
194.50 2.172 1000