59641-25-7

2-氯-3-吡咯烷-1,4-萘醌(59641-25-7)红外图谱(IR1)

产品名称:2-氯-3-吡咯烷-1,4-萘醌

CAS:59641-25-7

分子式:C14H12ClNO2

分子量: 261.7

Mass

MS-NW-9910          
2-chloro-3-(1-pyrrolidinyl)-1,4-naphthoquinone
C14H12ClNO2         (Mass of molecular ion:    261)

   Source Temperature: 220 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      18.0       1.6
      27.0       1.2
      28.0       1.8
      39.0       1.6
      41.0       2.2
      42.0       1.4
      43.0       6.0
      50.0       1.7
      51.0       1.1
      55.0       1.4
      56.0       1.5
      68.0       1.7
      70.0      20.1
      71.0       1.1
      74.0       1.3
      75.0       2.3
      76.0       4.8
      77.0       2.1
      80.0       1.0
      87.0       1.5
      88.0       1.2
      89.0       1.3
      99.0       2.6
     101.0       3.5
     102.0       1.4
     104.0       3.4
     105.0       5.7
     109.5       1.5
     114.0       3.5
     115.0       3.1
     126.0       1.1
     128.0       1.6
     129.0       4.5
     130.0       1.3
     135.0       2.8
     136.0       1.1
     137.0       1.0
     142.0       1.0
     143.0       1.8
     149.0       1.1
     154.0       2.2
     157.0      17.3
     158.0       2.3
     163.0       2.1
     164.0       1.3
     167.0       1.2
     169.0       1.5
     170.0       3.7
     171.0       7.6
     172.0       4.5
     178.0       1.4
     180.0       1.2
     191.0       2.0
     192.0       5.0
     193.0       1.4
     194.0       1.8
     196.0       1.6
     197.0       2.9
     198.0      16.8
     199.0       2.9
     205.0       1.9
     206.0      13.3
     207.0       2.5
     208.0       5.3
     209.0       2.0
     210.0       1.2
     218.0       2.2
     219.0       1.6
     220.0       3.2
     222.0       1.3
     223.0       3.0
     224.0       3.4
     225.0       2.7
     226.0      17.4
     227.0       5.6
     228.0       3.2
     232.0       2.1
     233.0      17.9
     234.0       3.2
     235.0       5.9
     260.0      16.8
     261.0     100.0
     262.0      21.7
     263.0      34.6
     264.0       5.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₂ Cl N O₂	0.036 g : 0.5 ml CDCl₃
2-chloro-3-(1-pyrrolidinyl)-1,4-naphthoquinone

    Assign.     Shift(ppm)

      A             8.078
      B             7.904
      C             7.670
      D             7.587
      E             3.970
      F             1.934

     Hz     ppm     Int.

   3233.52   8.091    257
   3232.18   8.088    259
   3225.95   8.072    273
   3225.46   8.071    271
   3224.61   8.069    274
   3163.09   7.915    249
   3161.74   7.912    250
   3155.40   7.896    288
   3154.05   7.893    279
   3074.22   7.693    145
   3072.88   7.689    145
   3066.77   7.674    324
   3065.43   7.671    300
   3059.20   7.655    210
   3057.86   7.652    183
   3039.31   7.605    222
   3037.96   7.602    214
   3031.86   7.587    316
   3030.52   7.583    297
   3024.29   7.568    133
   3022.95   7.564    120
   1593.51   3.988    358
   1590.70   3.981    331
   1589.48   3.978    366
   1586.67   3.971    960
   1583.98   3.964    362
   1582.76   3.961    322
   1579.96   3.954    360
    785.16   1.965     48
    784.06   1.962     44
    779.91   1.952    379
    776.12   1.942    436
    773.07   1.935   1000
    770.14   1.928    432
    766.36   1.918    364
    762.21   1.908     49
    761.23   1.905     49

in CDCl3

KBr disc

nujol mull

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