氢溴酸去甲猪毛菜碱(59709-57-8)红外图谱(IR2)

Mass

MS-NW-9899          
1-methyl-1,2,3,4-tetrahydro-6,7-isoquinolinediol hydrobromide
C10H13NO2 HBr       (Mass of molecular ion:    179)

   Source Temperature: 230 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      17.0       1.7
      18.0       9.0
      27.0       1.0
      28.0       2.5
      30.0       2.3
      39.0       1.9
      42.0       1.7
      51.0       2.4
      53.0       1.2
      54.0       1.0
      55.0       1.1
      56.0       1.5
      58.5       4.6
      59.0       1.5
      63.0       1.1
      64.5       1.1
      65.0       2.2
      65.5       2.2
      77.0       3.3
      78.0       1.0
      79.0       4.7
      80.0      14.4
      81.0       4.7
      81.5       4.0
      82.0      14.3
      89.0       1.5
      91.0       3.7
     103.0       2.3
     104.0       1.6
     105.0       1.0
     117.0       1.1
     118.0       1.3
     119.0       2.8
     123.0       1.4
     124.0       1.1
     131.0       2.4
     132.0       1.1
     133.0       1.9
     134.0       1.5
     135.0       2.0
     136.0       2.0
     137.0       7.0
     146.0       1.1
     147.0       2.6
     148.0       1.1
     149.0       6.3
     150.0       5.6
     162.0       3.9
     163.0       4.6
     164.0     100.0
     165.0      10.2
     175.0       1.4
     176.0       3.5
     177.0       2.5
     178.0      12.4
     179.0       5.4

Assign. Shift(ppm) A *1 9.31 B *1 9.0 C *1 8.91 D *2 6.630 E *2 6.563 F 4.40 G *3 3.37 J *3 3.22 K *4 2.88 L *4 2.79 M 1.513

     Hz     ppm     Int.

   3719.18   9.307     88
   3560.64   8.910     95
   2649.99   6.631    810
   2623.14   6.564    810
   1765.29   4.418     74
   1764.98   4.417     74
   1759.19   4.402    121
   1755.83   4.394    122
   1750.03   4.379     79
   1749.57   4.378     79
   1362.30   3.409     31
   1357.12   3.396     70
   1351.17   3.381    101
   1345.21   3.366    121
   1339.57   3.352    103
   1303.25   3.261     35
   1302.80   3.260     35
   1302.19   3.259     35
   1296.84   3.245     81
   1296.39   3.244     81
   1290.28   3.229    108
   1289.83   3.228    107
   1283.72   3.213     93
   1279.75   3.203     64
   1277.62   3.197     67
   1271.82   3.183     33
   1167.60   2.922     47
   1161.80   2.908     64
   1161.19   2.906     63
   1150.97   2.880    103
   1143.65   2.862    135
   1137.54   2.847     82
   1124.73   2.815     92
   1119.08   2.801    180
   1113.28   2.786     97
   1107.94   2.773     58
   1102.14   2.758     88
   1096.65   2.745     43
    608.06   1.522    998
    601.20   1.505   1000