6297-14-9

4-氨基-ALPHA-二乙胺-邻甲酚二盐酸盐(6297-14-9)质谱(MS)

产品名称:4-氨基-ALPHA-二乙胺-邻甲酚二盐酸盐

CAS:6297-14-9

分子式:C11H20Cl2N2O

分子量: 267.2

¹HNMR

IR1

IR2

Mass

MS-IW-0700          
4-amino-alpha-diethylamino-o-cresol dihydrochloride
C11H18N2O 2HCl      (Mass of molecular ion:    194)

   Source Temperature: 190 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      27.0       2.5
      28.0       4.9
      29.0       4.0
      30.0      20.8
      35.0       3.5
      36.0      51.2
      37.0       1.2
      38.0      17.1
      39.0       2.3
      40.0       1.0
      41.0       2.3
      42.0       3.6
      44.0      11.0
      46.0       1.5
      52.0       1.5
      53.0       1.5
      54.0       1.8
      56.0       2.5
      58.0      59.7
      59.0       2.3
      65.0       3.7
      66.0      11.5
      67.0       2.6
      72.0      25.4
      73.0      11.0
      74.0      75.3
      75.0       3.7
      77.0       2.9
      80.0       2.1
      86.0       3.3
      89.5       2.9
      92.0       3.1
      93.0      18.5
      94.0       5.9
      97.0       1.0
     106.0       1.0
     109.0       1.5
     120.0       1.1
     121.0     100.0
     122.0      30.8
     123.0      11.7
     135.0       1.2
     136.0       1.2
     165.0       1.4
     179.0       3.8
     193.0       1.5
     194.0      73.2
     195.0      10.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₁ H₁₈ N₂ O	0.037 g : 0.5 ml DMSO-d₆
4-amino-alpha-diethylamino-o-cresol dihydrochloride

    Assign.     Shift(ppm)

      A     *1     11.
      B            11.5
      C     *1     10.1
      D             7.557
      E             7.352
      F             7.194
      G             4.231
      J             3.07
      K             1.274

     Hz     ppm     Int.

   4184.25  10.470     39
   4039.74  10.109     26
   3021.88   7.562    216
   3019.13   7.555    228
   2944.58   7.368    116
   2941.84   7.362    108
   2935.79   7.346    151
   2933.23   7.340    149
   2879.01   7.204    266
   2870.40   7.183    224
   1691.18   4.232    293
   1229.78   3.078    174
   1229.41   3.077    174
   1229.05   3.076    174
   1225.75   3.068    179
   1225.20   3.066    178
    516.35   1.293    477
    509.20   1.275   1000
    501.88   1.256    464

KBr disc