63648-73-7

N-CBZ-D-谷氨酸(63648-73-7)红外图谱(IR1)

分子式:C13H15NO6

分子量: 281.26

InChI:InChI=1S/C13H15NO6/c15-11(16)7-6-10(12(17)18)14-13(19)20-8-9-4-2-1-3-5-9/h1-5,10H,6-8H2,(H,14,19)(H,15,16)(H,17,18)/t10-/m1/s1

InChIKey: PVFCXMDXBIEMQG-SNVBAGLBSA-N

Smiles:C(O)(=O)[C@@H](CCC(O)=O)NC(OCC1=CC=CC=C1)=O

¹HNMR

¹³CNMR

IR1

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₃ H₁₅ N O₆	0.031 g : 0.5 ml DMSO-d₆
N-benzyloxycarbonyl-D-glutamic acid

    Assign.     Shift(ppm)

      A            12.5
      B             7.61
      C             7.36
      D             7.33
      E             5.039
      F             4.007
      G             2.31
      J     *1      1.974
      K     *1      1.771

     Hz     ppm     Int.

   3048.20   7.628    128
   3040.30   7.608    134
   2955.68   7.396     34
   2953.97   7.392     30
   2946.28   7.373    306
   2942.64   7.364   1000
   2937.94   7.352    140
   2933.24   7.340    121
   2930.68   7.334    100
   2929.18   7.330     93
   2924.69   7.319    107
   2922.98   7.314     93
   2919.99   7.307     62
   2916.15   7.297     40
   2014.40   5.041    631
   1613.31   4.037     42
   1608.40   4.025     52
   1603.91   4.014     70
   1600.28   4.005     66
   1599.21   4.002     63
   1595.58   3.993     52
   1590.66   3.981     42
    933.59   2.337     72
    928.46   2.324     83
    925.68   2.317    140
    922.69   2.309    107
    920.98   2.305    102
    917.99   2.297     89
    914.78   2.289     79
    800.67   2.004     34
    795.12   1.990     52
    786.78   1.969     57
    781.66   1.956     46
    779.31   1.950     32
    718.83   1.799     32
    716.48   1.793     37
    716.06   1.792     37
    710.71   1.779     48
    709.43   1.776     49
    707.29   1.770     39
    705.16   1.765     39
    701.31   1.755     46
    695.54   1.741     33

in DMSO-d6