720-44-5

4-甲氧基二苯甲醇(720-44-5)红外图谱(IR2)

产品名称:4-甲氧基二苯甲醇

CAS:720-44-5

分子式:C14H14O2

分子量: 214.26

InChI:InChI=1S/C14H14O2/c1-16-13-9-7-12(8-10-13)14(15)11-5-3-2-4-6-11/h2-10,14-15H,1H3

InChIKey: BEGZWXVLBIZFKQ-UHFFFAOYSA-N

Smiles:C(C1C=CC=CC=1)(C1C=CC(OC)=CC=1)O

Mass

MS-IW-9744          
4-methoxybenzhydryl alcohol
C14H14O2            (Mass of molecular ion:    214)

   Source Temperature: 170 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      17.0       1.2
      18.0       6.1
      27.0       1.4
      28.0       1.3
      39.0       4.2
      50.0       3.2
      51.0       9.9
      52.0       1.7
      53.0       1.7
      55.0       1.7
      62.0       1.1
      63.0       5.1
      64.0       4.9
      65.0       4.9
      66.0       2.2
      74.0       1.3
      75.0       1.8
      76.0       5.2
      77.0      44.1
      78.0       7.9
      79.0       6.6
      82.0       1.4
      82.5       1.6
      83.0       1.0
      89.0       1.9
      91.0       5.7
      92.0       9.3
      93.0       4.3
      94.0       9.5
      98.0       1.6
      99.0       2.6
     102.0       1.2
     105.0      57.1
     106.0       5.8
     107.0       9.6
     108.0      34.5
     109.0      98.7
     110.0       7.7
     115.0       4.0
     120.0       1.1
     121.0      12.2
     122.0       1.2
     127.0       1.9
     128.0       2.8
     135.0     100.0
     136.0      18.7
     137.0      44.2
     138.0       4.0
     139.0       2.2
     141.0       2.5
     151.0       1.9
     152.0       8.7
     153.0      10.3
     154.0       4.4
     155.0       2.9
     165.0      12.0
     166.0       5.5
     167.0      13.7
     168.0       2.7
     169.0       1.7
     170.0       1.4
     181.0       5.6
     182.0       5.0
     183.0      13.0
     184.0       2.2
     185.0       1.1
     195.0       1.8
     196.0       2.1
     197.0      35.6
     198.0      53.3
     199.0       8.2
     211.0       1.8
     212.0      23.2
     213.0      19.9
     214.0      70.7
     215.0      10.7
     216.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₄ O₂	0.040 g : 0.5 ml CDCl₃
4-methoxybenzhydryl alcohol

    Assign.     Shift(ppm)

      A             7.34
      B             7.31
      C             7.24
      D             6.833
      E             5.737
      F             3.748

     Hz     ppm     Int.

   2938.60   7.353     50
   2936.52   7.348     71
   2934.69   7.344     39
   2934.33   7.343     38
   2930.05   7.332    207
   2928.47   7.328    186
   2927.61   7.326    178
   2926.76   7.324    197
   2924.56   7.318     44
   2920.65   7.309    137
   2919.80   7.306    193
   2917.97   7.302     72
   2913.82   7.291     44
   2911.87   7.287     71
   2901.98   7.262     35
   2899.66   7.256    215
   2899.29   7.255    213
   2897.71   7.251    119
   2896.24   7.247     51
   2890.87   7.234    265
   2888.06   7.227     42
   2884.52   7.218     51
   2738.04   6.852     35
   2735.23   6.845    251
   2733.03   6.839     79
   2728.52   6.828     79
   2726.32   6.822    223
   2294.56   5.742     87
   2291.14   5.733     85
   1498.05   3.749   1000

in CDCl3