7665-72-7

叔丁基缩水甘油基醚(7665-72-7)质谱(MS)

产品名称:叔丁基缩水甘油基醚

CAS:7665-72-7

分子式:C7H14O2

分子量: 130.18

InChI:InChI=1S/C7H14O2/c1-7(2,3)9-5-6-4-8-6/h6H,4-5H2,1-3H3

InChIKey: SFJRUJUEMVAZLM-UHFFFAOYSA-N

Smiles:O1CC1COC(C)(C)C

Mass

MS-IW-9299          
tert-butyl 2,3-epoxypropyl ether
C7H14O2             (Mass of molecular ion:    130)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.4
      27.0       7.7
      28.0       2.7
      29.0      44.0
      30.0       1.2
      31.0      16.3
      39.0       4.5
      41.0      22.7
      42.0       1.9
      43.0       6.2
      44.0       1.4
      45.0       1.2
      55.0       2.4
      56.0       7.7
      57.0     100.0
      58.0       4.4
      59.0      23.3
      73.0       1.7
     115.0      36.2
     116.0       2.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₄ O₂	0.05 ml : 0.5 ml CDCl₃
tert-butyl 2,3-epoxypropyl ether

    Assign.     Shift(ppm)

      A     *1      3.549
      B     *1      3.397
      C             3.099
      D             2.793
      E             2.614
      F             1.209

     Hz     ppm     Int.

   1426.64   3.570     66
   1422.85   3.561     68
   1415.89   3.543     91
   1412.11   3.534     93
   1365.11   3.416     79
   1359.74   3.403     85
   1354.37   3.389     57
   1349.00   3.376     63
   1243.77   3.113     32
   1242.68   3.110     49
   1240.97   3.106     35
   1239.99   3.103     52
   1238.65   3.100     53
   1237.18   3.096     49
   1235.96   3.093     37
   1234.50   3.089     46
   1233.28   3.086     32
   1120.73   2.805     83
   1116.70   2.795     86
   1115.60   2.792    107
   1111.57   2.782     88
   1047.97   2.623     90
   1045.29   2.616     89
   1042.85   2.610     81
   1040.16   2.603     78
    483.40   1.210   1000

in CDCl3