4-羟基-3-甲氧基苯甲酸己酯(84375-71-3)红外图谱(IR1)

Mass

MS-NW-7555          
hexyl vanillate
C14H20O4            (Mass of molecular ion:    252)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       3.3
      28.0       1.5
      29.0       4.1
      39.0       2.6
      41.0       7.4
      42.0       2.2
      43.0       6.0
      51.0       2.0
      52.0       3.9
      53.0       1.1
      55.0       4.4
      56.0       4.4
      63.0       1.0
      65.0       3.6
      67.0       1.6
      69.0       1.4
      77.0       1.8
      79.0       1.4
      80.0       1.8
      92.0       1.2
      93.0       2.6
      97.0       1.2
     108.0       4.1
     109.0       1.2
     120.0       1.0
     122.0       1.2
     123.0       7.8
     124.0       1.2
     125.0       2.1
     151.0      46.6
     152.0       5.2
     153.0      12.4
     154.0       1.4
     168.0     100.0
     169.0      14.0
     170.0       1.9
     181.0       1.1
     252.0      16.4
     253.0       2.9

Assign. Shift(ppm) A 7.633 B 7.555 C 6.940 D 6.4 E 4.289 F 3.895 G 1.75 J 1.49 to 1.24 K 0.91

     Hz     ppm     Int.

    689.50   7.699     92
    687.63   7.678    118
    681.31   7.608     93
    679.44   7.587    198
    677.31   7.563    223
    675.56   7.544    131
    625.19   6.981    198
    617.06   6.890    154
    390.75   4.363    108
    388.50   4.338     35
    388.19   4.335     35
    387.19   4.324     39
    384.31   4.292    258
    377.81   4.219    146
    349.06   3.898   1000
    165.19   1.845     35
    163.44   1.825     46
    162.44   1.814     43
    162.00   1.809     43
    161.31   1.802     44
    160.81   1.796     44
    160.31   1.790     45
    156.94   1.753     76
    153.75   1.717     53
    150.50   1.681     68
    146.75   1.639     41
    145.94   1.630     42
    145.56   1.626     40
    144.50   1.614     41
    144.38   1.613     41
    143.94   1.608     41
    143.38   1.601     42
    143.00   1.597     41
    141.88   1.585     37
    141.19   1.577     38
    140.63   1.571     38
    139.81   1.562     36
    138.94   1.552     36
    138.56   1.548     38
    136.94   1.530     44
    134.81   1.506     64
    134.44   1.502     65
    134.00   1.497     65
    133.69   1.493     66
    132.69   1.482     66
    129.69   1.449     85
    123.06   1.375    264
    121.25   1.354    251
    119.31   1.333    250
    111.38   1.244     65
    109.00   1.218     51
    106.94   1.195     34
    105.94   1.183     30
     86.50   0.966     97
     86.31   0.964     97
     85.00   0.950     90
     82.63   0.923    101
     80.44   0.899    262
     75.69   0.846     64
     74.25   0.830     68