880-09-1

二哌啶甲烷(880-09-1)红外图谱(IR1)

产品名称:二哌啶甲烷

CAS:880-09-1

分子式:C11H22N2

分子量: 182.31

InChI:InChI=1S/C11H22N2/c1-3-7-12(8-4-1)11-13-9-5-2-6-10-13/h1-11H2

InChIKey: LRKYLKBLUJXTFL-UHFFFAOYSA-N

Smiles:C(N1CCCCC1)N1CCCCC1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-8910          
dipiperidinomethane
C11H22N2            (Mass of molecular ion:    182)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.3
      27.0       3.8
      28.0       9.6
      29.0       9.5
      30.0       9.3
      39.0       3.5
      40.0       1.0
      41.0       9.7
      42.0      15.0
      43.0       9.9
      44.0      12.4
      53.0       1.4
      54.0       1.9
      55.0       8.8
      56.0      13.1
      57.0      11.1
      58.0       1.2
      67.0       2.1
      68.0       2.0
      69.0       2.8
      70.0       6.3
      82.0       1.7
      84.0      35.8
      85.0      19.1
      86.0       1.5
      94.0       1.4
      95.0       1.9
      96.0       3.9
      97.0       8.5
      98.0     100.0
      99.0       8.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₁ H₂₂ N₂	0.04 ml : 0.5 ml CDCl₃
dipiperidinomethane

    Assign.     Shift(ppm)

      A             2.828
      B          2.46 to 2.35
      C          1.67 to 1.33
     
     CHEMICALLY EXCHENGING SYSTEM.

     Hz     ppm     Int.

    255.31   2.851     35
    253.31   2.829   1000
    251.25   2.806     30
    218.94   2.445    251
    215.88   2.411    419
    210.38   2.350    376
    148.75   1.661     59
    147.94   1.652     54
    147.00   1.642     51
    143.13   1.599    166
    142.19   1.588    155
    133.50   1.491    479
    131.81   1.472    630
    130.63   1.459    448
    125.88   1.406     78
    123.63   1.381     60
    123.13   1.375     61
    120.75   1.349     40
    119.94   1.340     35
    119.50   1.335     36
    118.88   1.328     36
    118.44   1.323     35

in CDCl3