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90-45-9

9-氨基吖啶(90-45-9)质谱(MS)

产品名称:9-氨基吖啶

CAS:90-45-9

分子式:C13H10N2

分子量: 194.23

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    Mass

    MS-NW-7822          
    9-acridinamine
    C13H10N2            (Mass of molecular ion:    194)
    

       Source Temperature: 180 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          39.0       1.8
          50.0       1.2
          51.0       1.8
          63.0       1.8
          64.0       1.1
          65.0       2.0
          66.0       9.7
          69.5       1.6
          70.5       1.7
          75.0       1.7
          76.0       2.0
          77.0       2.5
          82.5       1.9
          83.0       1.6
          83.5       5.0
          84.0       1.3
          91.0       1.0
          96.0       1.1
          96.5       3.2
          97.0       8.3
          97.5       1.2
         102.0       1.9
         115.0       1.0
         129.0       1.8
         139.0       3.3
         140.0       4.2
         164.0       2.0
         165.0       1.3
         166.0       8.3
         167.0       5.2
         168.0       3.1
         192.0       5.0
         193.0      14.9
         194.0     100.0
         195.0      15.3
         196.0       1.1
    

400 MHz in DMSO-d6

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    1H NMR 399.65 MHz
    C13 H10 N2 0.040 g : 0.5 ml DMSO-d6
    9-acridinamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.473 B 7.901 C 7.685 D 7.353

         Hz     ppm     Int.
    

       3390.75   8.485    749
       3382.20   8.463    779
       3162.23   7.913    837
       3153.69   7.892   1000
       3078.49   7.703    484
       3071.53   7.686    655
       3063.23   7.665    434
       2946.04   7.372    474
       2938.60   7.353    641
       2930.91   7.334    418
    

in DMSO-d6

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KBr disc

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nujol mull

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