912-61-8

1,2,3,5-苯基苯(912-61-8)质谱(MS)

产品名称:1,2,3,5-苯基苯

CAS:912-61-8

分子式:C30H22

分子量: 382.5

¹HNMR

IR1

IR2

Mass

MS-NW-7729          
1,2,3,5-tetraphenylbenzene
C30H22              (Mass of molecular ion:    382)

   Source Temperature: 190 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      77.0       1.3
      91.0       2.0
      92.0       1.2
     138.0       1.1
     144.5       1.6
     150.0       2.0
     151.0       2.7
     151.5       1.3
     152.0       3.3
     156.5       1.2
     162.0       1.5
     163.0       2.4
     163.5       1.1
     168.5       2.2
     169.0       1.4
     169.5       2.7
     170.0       2.4
     170.5       1.6
     174.0       1.1
     175.0       3.8
     175.5       2.6
     176.0       3.2
     176.5       1.0
     177.0       1.4
     180.5       1.1
     181.5       3.1
     182.0       3.1
     182.5       2.0
     183.0       2.8
     183.5       1.4
     187.0       1.2
     188.0       1.3
     189.0       1.0
     191.0       3.3
     191.5       1.0
     202.0       1.0
     226.0       1.3
     236.0       2.0
     276.0       2.5
     277.0       1.2
     278.0       1.0
     289.0       7.4
     290.0       4.4
     291.0       4.7
     292.0       1.1
     300.0       2.5
     301.0       1.6
     302.0       7.5
     303.0       6.0
     304.0       5.4
     305.0       6.1
     306.0       1.6
     326.0       1.3
     328.0       1.0
     339.0       2.6
     340.0       1.1
     341.0       5.5
     342.0       1.7
     350.0       1.2
     351.0       1.1
     352.0       1.9
     353.0       1.8
     354.0       1.4
     363.0       2.3
     364.0       1.5
     365.0       6.3
     366.0       4.4
     367.0       3.6
     368.0       1.1
     376.0       1.3
     377.0       1.2
     378.0       1.2
     379.0       2.3
     380.0       1.7
     381.0      10.1
     382.0     100.0
     383.0      32.2
     384.0       5.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₃₀ H₂₂	0.036 g : 0.5 ml CDCl₃
1,2,3,5-tetraphenylbenzene

    Assign.     Shift(ppm)

      A             7.70
      B             7.682
      C             7.443
      D             7.356
      E          7.15 to 7.14
      F             6.98
      G             6.87

     Hz     ppm     Int.

   3081.91   7.712    165
   3080.57   7.709    213
   3078.61   7.704     82
   3073.49   7.691    246
   3072.39   7.688    246
   3070.07   7.682   1000
   2981.93   7.462    117
   2980.22   7.458     56
   2974.73   7.444    241
   2973.51   7.441    141
   2968.38   7.428     71
   2966.92   7.424    146
   2947.02   7.375     55
   2945.68   7.371     97
   2944.46   7.368     65
   2940.43   7.358     45
   2938.35   7.353    119
   2936.28   7.348     41
   2932.25   7.338     31
   2931.03   7.334     48
   2860.35   7.158    484
   2858.15   7.152    807
   2857.30   7.150    715
   2854.49   7.143    854
   2793.33   6.990    298
   2791.50   6.985    309
   2788.70   6.978    155
   2788.09   6.977    150
   2786.25   6.972    196
   2748.78   6.878    184
   2746.95   6.874    211
   2743.90   6.866    107
   2742.31   6.862    110
   2741.82   6.861    111
   2739.14   6.854    143

KBr disc

nujol mull