97674-02-7

三丁基(1-乙氧基乙烯)锡(97674-02-7)红外图谱(IR1)

产品名称:三丁基(1-乙氧基乙烯)锡

CAS:97674-02-7

分子式:C16H34OSn

分子量: 361.15

Mass

MS-NW-9651          
tributyl(1-ethoxyvinyl)stannane
C16H34OSn           (Mass of molecular ion:    362)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       3.6
      28.0       2.4
      29.0       8.4
      31.0       1.6
      39.0       2.2
      41.0       7.8
      42.0       1.0
      43.0       5.5
      44.0       1.4
      45.0       1.6
      55.0       2.0
      56.0       2.9
      57.0       4.7
      73.0       2.0
     116.0       2.5
     117.0      10.9
     118.0       8.9
     119.0      20.0
     120.0      12.1
     121.0      26.1
     122.0       2.3
     123.0       9.2
     125.0       4.8
     127.0      11.4
     128.0       1.0
     131.0       1.5
     132.0       1.0
     133.0       2.9
     134.0       1.5
     135.0       4.0
     137.0       1.7
     143.0       1.3
     145.0       3.3
     146.0       1.3
     147.0       4.2
     148.0       1.2
     149.0       4.4
     151.0       1.3
     159.0       1.6
     161.0       9.3
     162.0       4.6
     163.0      14.6
     164.0       5.3
     165.0      18.9
     167.0       4.3
     169.0       3.9
     171.0       3.5
     172.0       1.0
     173.0      10.5
     174.0       6.2
     175.0      46.0
     176.0      24.0
     177.0      70.5
     178.0      22.6
     179.0      75.2
     180.0       3.7
     181.0      13.5
     183.0      13.0
     187.0       1.3
     189.0       9.4
     190.0       5.4
     191.0      15.5
     192.0       5.7
     193.0      18.5
     195.0       3.3
     197.0       3.8
     199.0       2.4
     200.0       1.3
     201.0       4.3
     202.0       1.9
     203.0       5.9
     204.0       1.1
     205.0       2.7
     207.0       1.6
     219.0       4.7
     220.0       2.5
     221.0       7.1
     222.0       2.8
     223.0       8.9
     225.0       1.4
     227.0       3.2
     229.0       1.8
     230.0       6.3
     231.0      28.8
     232.0      24.5
     233.0      47.0
     234.0      30.7
     235.0      58.2
     236.0       6.9
     237.0       8.6
     238.0       3.0
     239.0      10.5
     240.0       1.0
     241.0       3.0
     243.0       3.2
     244.0       2.0
     245.0      44.7
     246.0      27.2
     247.0      76.3
     248.0      32.4
     249.0     100.0
     250.0       8.9
     251.0      15.1
     252.0       1.4
     253.0      17.9
     254.0       1.9
     255.0       3.0
     256.0       1.6
     257.0       4.4
     258.0       1.6
     259.0       4.5
     261.0       1.4
     263.0       1.2
     275.0       5.2
     276.0       3.2
     277.0       8.4
     278.0       3.8
     279.0      10.7
     280.0       1.2
     281.0       1.7
     283.0       2.4
     287.0       9.0
     288.0       6.2
     289.0      15.4
     290.0       7.6
     291.0      20.3
     292.0       2.7
     293.0       3.0
     295.0       3.6
     297.0       2.7
     299.0       1.9
     300.0       1.3
     301.0      39.0
     302.0      27.6
     303.0      69.2
     304.0      35.2
     305.0      91.3
     306.0      16.5
     307.0      13.5
     308.0       2.4
     309.0      16.3
     310.0       3.4
     311.0       4.1
     312.0       1.9
     313.0       5.6
     314.0       1.3
     315.0       3.7
     317.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₆ H₃₄ O Sn	0.05 ml : 0.5 ml CDCl₃
tributyl(1-ethoxyvinyl)stannane

    Assign.     Shift(ppm)

      A     *1      4.672
      B     *1      4.041
      C             3.693
      D             1.53
      E             1.324
      F             1.252
      G             0.943
      J             0.892

     Hz     ppm     Int.

   1868.16   4.675     91
   1866.46   4.671     95
   1616.09   4.044    117
   1614.38   4.040    117
   1486.33   3.720     51
   1479.37   3.702    145
   1472.41   3.685    147
   1465.45   3.667     51
    547.36   1.370     63
    540.04   1.352    163
    532.71   1.333    227
    524.90   1.314    230
    517.82   1.296    148
    510.62   1.278     58
    507.45   1.270    192
    500.49   1.253    361
    493.53   1.235    184
    384.77   0.963    310
    382.32   0.957     43
    379.15   0.949    132
    377.93   0.946    142
    376.59   0.943    260
    375.12   0.939    172
    372.44   0.932     52
    368.53   0.923    290
    363.65   0.910    550
    356.32   0.892   1000
    352.66   0.883     55
    349.12   0.874    501

in CDCl3