(±)-1,1,1-Trifluoro-2-butanaMine hydrochloride synthesis

1synthesis methods

Yield:31450-05-2 60 % Chromat. ，431-36-7 16 % Chromat. ，101054-93-7 24 % Chromat.

Reaction Conditions:

with sodium nitrite in perchloric acid;Product distribution;Mechanism;pH: 3.5 - 2.8;

References:

Gassen, Karl-Rudolf;Kirmse, Wolfgang [Chemische Berichte,1986,vol. 119,# 7,p. 2233 - 2248]

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